(1R)-1-C-allyl-N-(tert-butoxycarbonyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Base Information

Chemical Name:(1R)-1-C-allyl-N-(tert-butoxycarbonyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol
CAS No.:1354483-33-2
Molecular Formula:C₃₄H₄₁NO₅
Molecular Weight:543.703
Hs Code.:

Synonyms:(1R)-1-C-allyl-N-(tert-butoxycarbonyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

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Chemical Property of (1R)-1-C-allyl-N-(tert-butoxycarbonyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

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Technology Process of (1R)-1-C-allyl-N-(tert-butoxycarbonyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

There total 3 articles about (1R)-1-C-allyl-N-(tert-butoxycarbonyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1354483-32-1
(1R)-1-C-allyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

: 1354483-33-2
(1R)-1-C-allyl-N-(tert-butoxycarbonyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3.5h;
DOI:10.1080/07328303.2011.610544

Reference yield:

: 1354483-30-9
(1R)-1-C-allyl-N-naphth-2-ylmethyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

: 1354483-33-2
(1R)-1-C-allyl-N-(tert-butoxycarbonyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / dichloromethane

2: triethylamine / dichloromethane / 3.5 h / 0 - 20 °C

With methanol; triethylamine; In dichloromethane;
DOI:10.1080/07328303.2011.610544

Reference yield:

: 1-C-allyl-2,3,4-tri-O-benzyl-1-naphth-2-ylmethylamino-1-deoxy-D-xylitol

: 1354483-33-2
(1R)-1-C-allyl-N-(tert-butoxycarbonyl)-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-D-xylitol

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; methanesulfonyl chloride / 4 h / 100 °C / Molecular sieve

2: methanol / dichloromethane

3: triethylamine / dichloromethane / 3.5 h / 0 - 20 °C

With pyridine; methanol; methanesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1080/07328303.2011.610544