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C25H29N5O3S

Base Information
  • Chemical Name:C25H29N5O3S
  • CAS No.:1248504-26-8
  • Molecular Formula:C25H29N5O3S
  • Molecular Weight:479.603
  • Hs Code.:
C<sub>25</sub>H<sub>29</sub>N<sub>5</sub>O<sub>3</sub>S

Synonyms:C25H29N5O3S

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Chemical Property of C25H29N5O3S
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Technology Process of C25H29N5O3S

There total 8 articles about C25H29N5O3S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 9 steps
1.1: sodium hydride / diethyl ether; dimethyl sulfoxide; mineral oil / 3.58 h / 20 - 35 °C
2.1: water; sulfuric acid / 8 h / Reflux
3.1: triethylamine; diphenyl phosphoryl azide / toluene / 1.17 h / 20 - 100 °C
3.2: 3 h / 100 °C
4.1: water; lithium hydroxide / dimethyl sulfoxide / 2 h / 110 °C
5.1: acetone / 1 h / 20 °C
6.1: sodium hydroxide; water / methanol / 0.17 h / 50 °C
7.1: acetonitrile / 2 h / 50 °C
7.2: 2.5 h / 20 °C
8.1: water; ammonium chloride; iron / tetrahydrofuran; methanol / 3.5 h / Reflux
9.1: triethylamine; chlorophosphoric acid diphenyl ester / ethyl acetate / 0.83 h / 20 °C
With sulfuric acid; diphenyl phosphoryl azide; water; iron; sodium hydride; ammonium chloride; triethylamine; chlorophosphoric acid diphenyl ester; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide; ethyl acetate; acetone; toluene; acetonitrile; mineral oil;
Guidance literature:
Multi-step reaction with 7 steps
1.1: triethylamine; diphenyl phosphoryl azide / toluene / 1.17 h / 20 - 100 °C
1.2: 3 h / 100 °C
2.1: water; lithium hydroxide / dimethyl sulfoxide / 2 h / 110 °C
3.1: acetone / 1 h / 20 °C
4.1: sodium hydroxide; water / methanol / 0.17 h / 50 °C
5.1: acetonitrile / 2 h / 50 °C
5.2: 2.5 h / 20 °C
6.1: water; ammonium chloride; iron / tetrahydrofuran; methanol / 3.5 h / Reflux
7.1: triethylamine; chlorophosphoric acid diphenyl ester / ethyl acetate / 0.83 h / 20 °C
With diphenyl phosphoryl azide; water; iron; ammonium chloride; triethylamine; chlorophosphoric acid diphenyl ester; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dimethyl sulfoxide; ethyl acetate; acetone; toluene; acetonitrile;
Guidance literature:
Multi-step reaction with 8 steps
1.1: water; sulfuric acid / 8 h / Reflux
2.1: triethylamine; diphenyl phosphoryl azide / toluene / 1.17 h / 20 - 100 °C
2.2: 3 h / 100 °C
3.1: water; lithium hydroxide / dimethyl sulfoxide / 2 h / 110 °C
4.1: acetone / 1 h / 20 °C
5.1: sodium hydroxide; water / methanol / 0.17 h / 50 °C
6.1: acetonitrile / 2 h / 50 °C
6.2: 2.5 h / 20 °C
7.1: water; ammonium chloride; iron / tetrahydrofuran; methanol / 3.5 h / Reflux
8.1: triethylamine; chlorophosphoric acid diphenyl ester / ethyl acetate / 0.83 h / 20 °C
With sulfuric acid; diphenyl phosphoryl azide; water; iron; ammonium chloride; triethylamine; chlorophosphoric acid diphenyl ester; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dimethyl sulfoxide; ethyl acetate; acetone; toluene; acetonitrile;
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