1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbothioamide

Base Information

Chemical Name:1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbothioamide
CAS No.:135656-56-3
Molecular Formula:C₁₅H₁₄N₆O₃S
Molecular Weight:358.381
Hs Code.:

Synonyms:1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbothioamide

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Chemical Property of 1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbothioamide

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Technology Process of 1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbothioamide

There total 3 articles about 1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 135656-55-2
1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbonitrile

: 135656-56-3
1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbothioamide

Guidance literature:: With ammonium hydroxide; hydrogen sulfide; In water; for 48h; Ambient temperature;
DOI:10.1002/ardp.19913240713

Reference yield:

: 83-07-8
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

: 135656-56-3
1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaNO₂, 2.) NaOAc / 1.) H₂O, 0 deg C, 1 h, 2.) 0-5 deg C, 5 d

2: 90 percent / Na₂CO₃ / H₂O / 0.5 h / Heating

3: 85 percent / H₂S, 25percent NH₃ / H₂O / 48 h / Ambient temperature

With ammonium hydroxide; hydrogen sulfide; sodium acetate; sodium carbonate; sodium nitrite; In water;
DOI:10.1002/ardp.19913240713

Reference yield:

: 135656-54-1
ethyl-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-ylhydrazonocyanoacetylcarbamate

: 135656-56-3
1-(1-phenyl-2,3-dimethyl-5-oxo-2,5-dihydropyrazol-4-yl)-6-azauracil-5-carbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / Na₂CO₃ / H₂O / 0.5 h / Heating

2: 85 percent / H₂S, 25percent NH₃ / H₂O / 48 h / Ambient temperature

With ammonium hydroxide; hydrogen sulfide; sodium carbonate; In water;
DOI:10.1002/ardp.19913240713