11-(4-fluorophenyl)undecanoic acid

Base Information

Chemical Name:11-(4-fluorophenyl)undecanoic acid
CAS No.:1258638-45-7
Molecular Formula:C₁₇H₂₅FO₂
Molecular Weight:280.383
Hs Code.:

Synonyms:11-(4-fluorophenyl)undecanoic acid

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Chemical Property of 11-(4-fluorophenyl)undecanoic acid

Chemical Property:

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Technology Process of 11-(4-fluorophenyl)undecanoic acid

There total 4 articles about 11-(4-fluorophenyl)undecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 11-(4-fluorophenyl)undec-9-ynoic acid

: 1258638-45-7
11-(4-fluorophenyl)undecanoic acid

Guidance literature:: With 10 wt% Pd(OH)2 on carbon; hydrogen; acetic acid; In methanol; at 20 ℃; for 17h;
DOI:10.1016/j.carres.2018.11.005

Reference yield:

: 1354747-55-9
C₁₇H₂₁FO₂

: 1258638-45-7
11-(4-fluorophenyl)undecanoic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; acetic acid; In methanol; at 20 ℃; for 48h;
DOI:10.1021/ol2032448

Reference yield:

: 352-34-1
4-fluoro-1-iodobenzene

: 1258638-45-7
11-(4-fluorophenyl)undecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 50 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen; acetic acid / methanol / 48 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium 10% on activated carbon; hydrogen; acetic acid; triethylamine; In methanol; 1: Sonogashira coupling;
DOI:10.1021/ol2032448