Technology Process of C16H22O3
There total 4 articles about C16H22O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C19H30O2Si;
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 0 ℃;
With
hydrogenchloride; water;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1016/j.tetlet.2012.01.058
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-butyllithium / tetrahydrofuran / -30 °C
1.2: -30 °C
2.1: Crabtree's catalyst; hydrogen / 1,2-dichloro-ethane / 80 °C
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C
3.2: -78 - 20 °C
4.1: triethylamine / dichloromethane / 0 °C
5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
5.2: 20 °C
With
n-butyllithium; oxalyl dichloride; Crabtree's catalyst; hydrogen; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
1.1: Wittig reaction / 1.2: Wittig reaction / 3.1: Swern oxidation / 3.2: Swern oxidation / 5.1: Rubottom oxidation / 5.2: Rubottom oxidation;
DOI:10.1016/j.tetlet.2012.01.058
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C
1.2: -78 - 20 °C
2.1: triethylamine / dichloromethane / 0 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C
3.2: 20 °C
With
oxalyl dichloride; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
1.1: Swern oxidation / 1.2: Swern oxidation / 3.1: Rubottom oxidation / 3.2: Rubottom oxidation;
DOI:10.1016/j.tetlet.2012.01.058
