benzyl 4-[2'-hydroxy-4'-methoxy-6'-(2''-oxoheptyl)benzoyloxy]-2-methoxy-6-propylbenzoate

Base Information

Chemical Name:benzyl 4-[2'-hydroxy-4'-methoxy-6'-(2''-oxoheptyl)benzoyloxy]-2-methoxy-6-propylbenzoate
CAS No.:176447-90-8
Molecular Formula:C₃₃H₃₈O₈
Molecular Weight:562.66
Hs Code.:

Synonyms:benzyl 4-[2'-hydroxy-4'-methoxy-6'-(2''-oxoheptyl)benzoyloxy]-2-methoxy-6-propylbenzoate

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Chemical Property of benzyl 4-[2'-hydroxy-4'-methoxy-6'-(2''-oxoheptyl)benzoyloxy]-2-methoxy-6-propylbenzoate

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Technology Process of benzyl 4-[2'-hydroxy-4'-methoxy-6'-(2''-oxoheptyl)benzoyloxy]-2-methoxy-6-propylbenzoate

There total 3 articles about benzyl 4-[2'-hydroxy-4'-methoxy-6'-(2''-oxoheptyl)benzoyloxy]-2-methoxy-6-propylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 176447-88-4
benzyl 4-{2'-hydroxy-4'-methoxy-6'-[(2''-pentyl-1'',3''-dioxolan-2''-yl)methyl]benzoyloxy}-2-methoxy-6-propylbenzoate

: 176447-90-8
benzyl 4-[2'-hydroxy-4'-methoxy-6'-(2''-oxoheptyl)benzoyloxy]-2-methoxy-6-propylbenzoate

Guidance literature:: With hydrogenchloride; In methanol; for 2h; Ambient temperature;
DOI:10.1071/ch9960159

Reference yield:

: 176447-87-3
2-Hydroxy-4-methoxy-6-(2-pentyl-[1,3]dioxolan-2-ylmethyl)-benzoic acid

: 176447-90-8
benzyl 4-[2'-hydroxy-4'-methoxy-6'-(2''-oxoheptyl)benzoyloxy]-2-methoxy-6-propylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / N,N'-dicyclohexylcarbodiimide / toluene / 0.7 h / Ambient temperature

2: 81 percent / 5M HCl / methanol / 2 h / Ambient temperature

With hydrogenchloride; dicyclohexyl-carbodiimide; In methanol; toluene;
DOI:10.1071/ch9960159

Reference yield:

: 176447-86-2
ethyl 2-hydroxy-4-methoxy-6-<(2'-pentyl-1',3'-dioxolan-2'-yl)methyl>benzoate

: 176447-90-8
benzyl 4-[2'-hydroxy-4'-methoxy-6'-(2''-oxoheptyl)benzoyloxy]-2-methoxy-6-propylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydroxide; 2.) tartaric acid / 1.) water, dimethyl sulfoxide, 91 degC, 16 h; 2.) water, 0 degC

2: 84 percent / N,N'-dicyclohexylcarbodiimide / toluene / 0.7 h / Ambient temperature

3: 81 percent / 5M HCl / methanol / 2 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; tartaric acid; dicyclohexyl-carbodiimide; In methanol; toluene;
DOI:10.1071/ch9960159