tert-butyl (S)-(3-(3-((tert-butyldimethylsilyl)oxy)phenyl)but-3-en-2-yl)carbamate

Base Information

Chemical Name:tert-butyl (S)-(3-(3-((tert-butyldimethylsilyl)oxy)phenyl)but-3-en-2-yl)carbamate
CAS No.:1254224-06-0
Molecular Formula:C₂₁H₃₅NO₃Si
Molecular Weight:377.599
Hs Code.:

Synonyms:tert-butyl (S)-(3-(3-((tert-butyldimethylsilyl)oxy)phenyl)but-3-en-2-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (S)-(3-(3-((tert-butyldimethylsilyl)oxy)phenyl)but-3-en-2-yl)carbamate

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Technology Process of tert-butyl (S)-(3-(3-((tert-butyldimethylsilyl)oxy)phenyl)but-3-en-2-yl)carbamate

There total 1 articles about tert-butyl (S)-(3-(3-((tert-butyldimethylsilyl)oxy)phenyl)but-3-en-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1254223-99-8
C₁₆H₂₅N₃O₄S

: 65423-56-5
1-bromo-3-[(tert-butyldimethylsilyl)oxy]benzene

: 1254224-06-0
tert-butyl (S)-(3-(3-((tert-butyldimethylsilyl)oxy)phenyl)but-3-en-2-yl)carbamate

Guidance literature:: C₁₆H₂₅N₃O₄S; With water; palladium diacetate; lithium tert-butoxide; XPhos; In 1,4-dioxane; for 0.0166667h; Inert atmosphere;

1-bromo-3-[(tert-butyldimethylsilyl)oxy]benzene; In 1,4-dioxane; at 110 ℃; for 4h; optical yield given as %ee; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201003450