3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile)

Base Information

• Chemical Name: 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile)
• CAS No.: 161061-17-2
• Molecular Formula: C₂₅H₂₉N₇O₅
• Molecular Weight: 507.549

Synonyms:3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile)

Chemical Property of 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile)

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Technology Process of 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile)

There total 1 articles about 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

α-bromo-(2-methoxy-5-nitrophenyl)acetic acid, methyl ester + 3,9-bis(methylenenitrile)-3,6,9,15-teraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene (160981-97-5) → 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile) (161061-17-2)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 20h;

Reference yield: 98.3%

3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile) (161061-17-2) → 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid (174406-14-5)

Guidance literature:

With hydrogenchloride; water; at 100 ℃; for 2h; Heating / reflux;

upstream raw materials:

3,9-bis(methylenenitrile)-3,6,9,15-teraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene

Downstream raw materials:

3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid

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