N-2-(3-benzyloxy-4-methoxyphenyl)ethyl-3-(3',4'-dimethoxyphenyl)propionamide

Base Information

• Chemical Name: N-2-(3-benzyloxy-4-methoxyphenyl)ethyl-3-(3',4'-dimethoxyphenyl)propionamide
• CAS No.: 65899-35-6
• Molecular Formula: C₂₇H₃₁NO₅
• Molecular Weight: 449.547

Synonyms:N-2-(3-benzyloxy-4-methoxyphenyl)ethyl-3-(3',4'-dimethoxyphenyl)propionamide

Chemical Property of N-2-(3-benzyloxy-4-methoxyphenyl)ethyl-3-(3',4'-dimethoxyphenyl)propionamide

Chemical Property:

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Technology Process of N-2-(3-benzyloxy-4-methoxyphenyl)ethyl-3-(3',4'-dimethoxyphenyl)propionamide

There total 2 articles about N-2-(3-benzyloxy-4-methoxyphenyl)ethyl-3-(3',4'-dimethoxyphenyl)propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

3-benzyloxy-4-methoxyphenylethylamine (36455-21-7) + 3,4-methoxycinnamic acid (2107-70-2) → N-2-(3-benzyloxy-4-methoxyphenyl)ethyl-3-(3',4'-dimethoxyphenyl)propionamide (65899-35-6)

Guidance literature:

at 160 ℃; for 6h;

DOI:10.1248/cpb.35.3666

Reference yield:

→ N-2-(3-benzyloxy-4-methoxyphenyl)ethyl-3-(3',4'-dimethoxyphenyl)propionamide (65899-35-6)

Guidance literature:

3-Benzyloxy-4-methoxyphenethylamin, 3,4-Dimethoxyphenylpropionsaeure 2a;

DOI:10.1021/jo00406a051

Reference yield: 82.0%

N-2-(3-benzyloxy-4-methoxyphenyl)ethyl-3-(3',4'-dimethoxyphenyl)propionamide (65899-35-6) → 6-benzyloxy-3,4-dihydro-7-methoxy-1-(2-(3',4'-dimethoxyphenyl)ethyl)isoquinoline hydrochloride (65899-37-8)

Guidance literature:

With trichlorophosphate; In dichloromethane; for 3h; Heating;

DOI:10.1248/cpb.35.3666

upstream raw materials:

3-benzyloxy-4-methoxyphenylethylamine

3,4-methoxycinnamic acid

Downstream raw materials:

6-benzyloxy-3,4-dihydro-7-methoxy-1-(2-(3',4'-dimethoxyphenyl)ethyl)isoquinoline hydrochloride

1,2,3,4-tetrahydro-6-hydroxy-7-methoxy-1-(2-(3',4'-dimethoxyphenyl)ethyl)-2-methylisoquinoline

Acetic acid 1-[2-(3,4-dimethoxy-phenyl)-ethyl]-7-methoxy-2-methyl-6-oxo-1,2,3,4,6,7-hexahydro-isoquinolin-7-yl ester

Acetic acid 1-[2-(3,4-dimethoxy-phenyl)-ethyl]-6-hydroxy-7-methoxy-2-methyl-1,2,3,4-tetrahydro-isoquinolin-4-yl ester

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