C₄₈H₄₆O₇

Base Information

Chemical Name:C₄₈H₄₆O₇
CAS No.:1413373-50-8
Molecular Formula:C₄₈H₄₆O₇
Molecular Weight:734.889
Hs Code.:

C<sub>48</sub>H<sub>46</sub>O<sub>7</sub>

Synonyms:C₄₈H₄₆O₇

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Chemical Property of C₄₈H₄₆O₇

Chemical Property:

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Technology Process of C₄₈H₄₆O₇

There total 12 articles about C₄₈H₄₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1413373-48-4
C₄₈H₄₈O₇

: 1413373-50-8
C₄₈H₄₆O₇

Guidance literature:: With Dess-Martin periodane; at 20 ℃;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1413373-50-8
C₄₈H₄₆O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: L-Selectride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

5.2: 0.25 h

6.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 0.5 h / 0 °C / Inert atmosphere

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 3 h / 0 - 20 °C

8.1: Dess-Martin periodane / 20 °C

With pyridine; oxalyl dichloride; tributylphosphine; dimethylsulfide borane complex; L-Selectride; Dess-Martin periodane; dimethyl sulfoxide; L-proline; 1,1'-azodicarbonyl-dipiperidine; trichlorophosphate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 6.1: Mitsunobu reaction;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 1413373-50-8
C₄₈H₄₆O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 0 °C

1.3: cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

5.1: L-Selectride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

5.2: 0.25 h

6.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 0.5 h / 0 °C / Inert atmosphere

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 3 h / 0 - 20 °C

8.1: Dess-Martin periodane / 20 °C

With sodium tetrahydroborate; n-butyllithium; tributylphosphine; dimethylsulfide borane complex; L-Selectride; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; trifluoroacetic anhydride; 1,1'-azodicarbonyl-dipiperidine; 18-crown-6 ether; In tetrahydrofuran; hexane; dichloromethane; toluene; 6.1: Mitsunobu reaction;