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trans-Mo(N2)2(Et2PC2H4PPh2)2

Base Information
  • Chemical Name:trans-Mo(N2)2(Et2PC2H4PPh2)2
  • CAS No.:73534-22-2
  • Molecular Formula:C36H48MoN4P4
  • Molecular Weight:756.639
  • Hs Code.:
trans-Mo(N<sub>2</sub>)2(Et<sub>2</sub>PC<sub>2</sub>H<sub>4</sub>PPh<sub>2</sub>)2

Synonyms:trans-Mo(N2)2(Et2PC2H4PPh2)2

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Chemical Property of trans-Mo(N2)2(Et2PC2H4PPh2)2
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Technology Process of trans-Mo(N2)2(Et2PC2H4PPh2)2

There total 1 articles about trans-Mo(N2)2(Et2PC2H4PPh2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With Na/Hg; N2; In tetrahydrofuran; under N2; portionwise addn. of MoCl5 to soln. of ligand, addn. of 1% Na/Hg amalgam, stirred for 1 day, settled undisturbed overnight; supernatant syringed off, remaining suspension filtered (Celite), reaction flask and filter cake washed (C6H6), combined solns. evapd. (vac.), dissolved (C6H6), filtered (Celite), washed (benzene), oil solidified on stirring;
Guidance literature:
With ethyl acetate; In toluene; under Ar; refluxed for 40 min, soln. turned brown-purple; not isolated;
Guidance literature:
With N2; ethyl acetate; In toluene; refluxed under N2; solvent removed partially, addn. of MeOH;
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