Carbamic acid, [(1S)-1-(hydroxymethyl)-3-methyl-3-butenyl]-, 1,1-dimethylethyl

Base Information

Chemical Name:Carbamic acid, [(1S)-1-(hydroxymethyl)-3-methyl-3-butenyl]-, 1,1-dimethylethyl
CAS No.:666718-78-1
Molecular Formula:C11H21NO3
Molecular Weight:215.28934
Hs Code.:
Mol file:666718-78-1.mol

Synonyms:Carbamic acid, [(1S)-1-(hydroxymethyl)-3-methyl-3-butenyl]-, 1,1-dimethylethyl

Suppliers and Price of Carbamic acid, [(1S)-1-(hydroxymethyl)-3-methyl-3-butenyl]-, 1,1-dimethylethyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [(1S)-1-(hydroxymethyl)-3-methyl-3-butenyl]-, 1,1-dimethylethyl

Chemical Property:

PSA：58.56000
LogP:2.22910

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Carbamic acid, [(1S)-1-(hydroxymethyl)-3-methyl-3-butenyl]-, 1,1-dimethylethyl

There total 5 articles about Carbamic acid, [(1S)-1-(hydroxymethyl)-3-methyl-3-butenyl]-, 1,1-dimethylethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: C₁₅H₂₅NO₆

: 666718-78-1
tert-butyl 1-(hydroxymethyl)-3-methylbut-3-enylcarbamate

Guidance literature:: With sodium tetrahydroborate; In water; at 0 ℃;
DOI:10.1016/j.bmcl.2003.09.088

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 87325-47-1
(2S)-2-tert-butoxycarbonylamino-4-methyl-4-pentenoic acid

: 666718-78-1
tert-butyl 1-(hydroxymethyl)-3-methylbut-3-enylcarbamate

Guidance literature:: di-tert-butyl dicarbonate; (2S)-2-tert-butoxycarbonylamino-4-methyl-4-pentenoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -10 ℃; for 0.5h;

With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 - 20 ℃;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 666718-78-1
tert-butyl 1-(hydroxymethyl)-3-methylbut-3-enylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH / dioxane / 20 °C

2: NEt₃ / tetrahydrofuran / -10 °C

3: 45 percent / NaBH₄ / H₂O / 0 °C

With sodium hydroxide; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1016/j.bmcl.2003.09.088