C₅₉H₅₉N₃O₈

Base Information

Chemical Name:C₅₉H₅₉N₃O₈
CAS No.:1338645-89-8
Molecular Formula:C₅₉H₅₉N₃O₈
Molecular Weight:938.133
Hs Code.:

C<sub>59</sub>H<sub>59</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₅₉H₅₉N₃O₈

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Chemical Property of C₅₉H₅₉N₃O₈

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Technology Process of C₅₉H₅₉N₃O₈

There total 13 articles about C₅₉H₅₉N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1338645-88-7
C₄₃H₄₄N₂O₇

: 962-39-0
L-Phenylalanine benzyl ester

: 1338645-89-8
C₅₉H₅₉N₃O₈

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ol202573s

Reference yield:

: C₂₉H₃₃NO₄

: 1338645-89-8
C₅₉H₅₉N₃O₈

Guidance literature:: Multi-step reaction with 5 steps

1: sodium periodate / acetone; toluene / 0.5 h

2: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

4: 1,4-diaza-bicyclo[2.2.2]octane; sodium periodate / tetrahydrofuran; water / 0.17 h

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

With 1,4-diaza-bicyclo[2.2.2]octane; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 2: Pinnick oxidation;
DOI:10.1021/ol202573s

Reference yield:

: C₂₆H₂₇NO₃

: 1338645-89-8
C₅₉H₅₉N₃O₈

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine / dichloromethane; toluene / -78 - 0 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / -78 - 0 °C

3: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; toluene / 5 h

4: sodium periodate / acetone; toluene / 0.5 h

5: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

7: 1,4-diaza-bicyclo[2.2.2]octane; sodium periodate / tetrahydrofuran; water / 0.17 h

8: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; boron trifluoride diethyl etherate; water; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 5: Pinnick oxidation;
DOI:10.1021/ol202573s