4-methoxybenzyl 6β-iodopenicillanate

Base Information

• Chemical Name: 4-methoxybenzyl 6β-iodopenicillanate
• CAS No.: 75722-79-1
• Molecular Formula: C₁₆H₁₈INO₄S
• Molecular Weight: 447.294

Synonyms:4-methoxybenzyl 6β-iodopenicillanate

Chemical Property of 4-methoxybenzyl 6β-iodopenicillanate

Chemical Property:

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Technology Process of 4-methoxybenzyl 6β-iodopenicillanate

There total 7 articles about 4-methoxybenzyl 6β-iodopenicillanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-methoxybenzyl 6α-trifloxypenicillanate (75722-78-0) → 4-methoxybenzyl 6β-iodopenicillanate (75722-79-1)

Guidance literature:

With sodium iodide; In acetone; for 46h; Ambient temperature;

DOI:10.1016/0040-4039(80)88017-8

Reference yield:

6-alpha-trifluorosulfonyloxypenicillanic acid 4-methoxybenzyl ester → 4-methoxybenzyl 6β-iodopenicillanate (75722-79-1)

Guidance literature:

With sodium iodide; In acetone;

Reference yield:

6,6-diiodopenicillanic acid 4-methoxybenzyl ester → 4-methoxybenzyl 6β-iodopenicillanate (75722-79-1)

Guidance literature:

upstream raw materials:

4-methoxybenzyl 6α-trifloxypenicillanate

6-α-hydroxypenicillanic acid

4-methoxybenzyl 6α-hydroxypenicillanate

p-methoxybenzyl chloride

Downstream raw materials:

6β-iodopenicillanic acid

(5R,6S)-6-(1,2-Dihydroxy-1-methyl-ethyl)-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid 4-methoxy-benzyl ester

(5R,6S)-6-((R)-4-Methyl-2-oxo-[1,3]dioxolan-4-yl)-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-methoxy-benzyl ester

p-methoxybenzyl (5R,6S)-6-(4-methyl-2-oxo-1,3-dioxolan-4-yl)penicillanate S-oxide

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