isopropyl 2-(4-bromophenyl)-2-diazoacetate

Base Information

Chemical Name:isopropyl 2-(4-bromophenyl)-2-diazoacetate
CAS No.:1432320-21-2
Molecular Formula:C₁₁H₁₁BrN₂O₂
Molecular Weight:283.125
Hs Code.:

Synonyms:isopropyl 2-(4-bromophenyl)-2-diazoacetate

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Chemical Property of isopropyl 2-(4-bromophenyl)-2-diazoacetate

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Technology Process of isopropyl 2-(4-bromophenyl)-2-diazoacetate

There total 3 articles about isopropyl 2-(4-bromophenyl)-2-diazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 89819-73-8
isopropyl 2-(4-bromophenyl)acetate

: 1432320-21-2
isopropyl 2-(4-bromophenyl)-2-diazoacetate

Guidance literature:: With 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201901343

Reference yield: 74.0%

: 67-63-0,8013-70-5
isopropyl alcohol

: 1878-68-8
2-(4-bromophenyl)-acetic acid

: 1432320-21-2
isopropyl 2-(4-bromophenyl)-2-diazoacetate

Guidance literature:: isopropyl alcohol; 2-(4-bromophenyl)-acetic acid; With sulfuric acid; at 90 ℃; for 12h;

With 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 12h;
DOI:10.1002/anie.201608937

Reference yield:

: 1878-68-8
2-(4-bromophenyl)-acetic acid

: 1432320-21-2
isopropyl 2-(4-bromophenyl)-2-diazoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 83 °C / Inert atmosphere

2: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0 - 20 °C / Inert atmosphere

With sulfuric acid; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;
DOI:10.1002/adsc.201901343