carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester

Base Information

Chemical Name:carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester
CAS No.:361196-94-3
Molecular Formula:C₂₄H₁₉BrO₆
Molecular Weight:483.315
Hs Code.:

Synonyms:carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester

Suppliers and Price of carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester

There total 7 articles about carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 79-22-1
methyl chloroformate

: 361196-93-2
3-[3-bromo-2-(4-methoxybenzyloxy)-phenyl]-3H-benzofuran-2-one

: 361196-94-3
carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ol016097r

Reference yield:

: 59214-70-9
3-bromobenzofuran

: 361196-94-3
carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / BuLi

2: 65 percent / Pd(dppf)Cl₂

3: 66 percent / CH₃CO₃H / CH₂Cl₂; acetic acid; H₂O / 48 h

4: 97 percent / NEt₃ / tetrahydrofuran / 0 - 20 °C

With peracetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; n-butyllithium; triethylamine; In tetrahydrofuran; dichloromethane; water; acetic acid;
DOI:10.1021/ol016097r

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 361196-94-3
carbonic acid 3-[3-bromo-2-(4-methoxy-benzyloxy)-phenyl]-benzofuran-2-yl ester methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaH / dimethylformamide / 24 h / 20 °C

2: 66 percent / CH₃CO₃H / CH₂Cl₂; acetic acid; H₂O / 48 h

3: 97 percent / NEt₃ / tetrahydrofuran / 0 - 20 °C

With peracetic acid; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ol016097r