2,3:4,5-di-O-isopropylidene-1-[4-(benzyloxycarbonylamino)-piperidin-1-yl]-1-deoxy-β-D-fructopyranose

Base Information

Chemical Name:2,3:4,5-di-O-isopropylidene-1-[4-(benzyloxycarbonylamino)-piperidin-1-yl]-1-deoxy-β-D-fructopyranose
CAS No.:1187321-38-5
Molecular Formula:C₂₅H₃₆N₂O₇
Molecular Weight:476.57
Hs Code.:

Synonyms:2,3:4,5-di-O-isopropylidene-1-[4-(benzyloxycarbonylamino)-piperidin-1-yl]-1-deoxy-β-D-fructopyranose

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Chemical Property of 2,3:4,5-di-O-isopropylidene-1-[4-(benzyloxycarbonylamino)-piperidin-1-yl]-1-deoxy-β-D-fructopyranose

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Technology Process of 2,3:4,5-di-O-isopropylidene-1-[4-(benzyloxycarbonylamino)-piperidin-1-yl]-1-deoxy-β-D-fructopyranose

There total 2 articles about 2,3:4,5-di-O-isopropylidene-1-[4-(benzyloxycarbonylamino)-piperidin-1-yl]-1-deoxy-β-D-fructopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74925-15-8
2,3:4,5-di-O-isopropylidene-1-O-(trifluoromethanesulfonyl)-β-D-fructopyranose

: 182223-54-7
piperidin-4-ylcarbamic acid benzyl ester

: 1187321-38-5
2,3:4,5-di-O-isopropylidene-1-[4-(benzyloxycarbonylamino)-piperidin-1-yl]-1-deoxy-β-D-fructopyranose

Guidance literature:: piperidin-4-ylcarbamic acid benzyl ester; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 0.25h;

2,3:4,5-di-O-isopropylidene-1-O-(trifluoromethanesulfonyl)-β-D-fructopyranose; In acetonitrile; for 4h; Reflux;

Reference yield:

: 20880-92-6
2,3;4,5-di-O-isopropylidene-β-D-fructopyranose

: 1187321-38-5
2,3:4,5-di-O-isopropylidene-1-[4-(benzyloxycarbonylamino)-piperidin-1-yl]-1-deoxy-β-D-fructopyranose

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0.25 h / 20 °C

2.2: 4 h / Reflux

With pyridine; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;