3-phenylpropyl 2,4,6-triisopropylbenzoate

Base Information

Chemical Name:3-phenylpropyl 2,4,6-triisopropylbenzoate
CAS No.:1338073-31-6
Molecular Formula:C₂₅H₃₄O₂
Molecular Weight:366.544
Hs Code.:

Synonyms:3-phenylpropyl 2,4,6-triisopropylbenzoate

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Chemical Property of 3-phenylpropyl 2,4,6-triisopropylbenzoate

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Technology Process of 3-phenylpropyl 2,4,6-triisopropylbenzoate

There total 2 articles about 3-phenylpropyl 2,4,6-triisopropylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 122-97-4
3-Phenyl-1-propanol

: 49623-71-4
2,4,6-triisopropylbenzoic acid

: 1338073-31-6
3-phenylpropyl 2,4,6-triisopropylbenzoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 4.5h;
DOI:10.1002/anie.201611273

Reference yield: 94.0%

: 122-97-4
3-Phenyl-1-propanol

: 57199-00-5
2,4,6-triisopropylbenzoyl chloride

: 1338073-31-6
3-phenylpropyl 2,4,6-triisopropylbenzoate

Guidance literature:: 3-Phenyl-1-propanol; With sodium hydride; In tetrahydrofuran; mineral oil; for 0.166667h; Inert atmosphere;

2,4,6-triisopropylbenzoyl chloride; In tetrahydrofuran; mineral oil; at 80 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1039/c2ob06975j

Reference yield: 97.0%

: 126689-01-8
cyclopropylboronic acid pinacol ester

: 1338073-31-6
3-phenylpropyl 2,4,6-triisopropylbenzoate

: 1338073-36-1
2-(1-cyclopropyl-3-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 3-phenylpropyl 2,4,6-triisopropylbenzoate; With sec.-butyllithium; (-)-sparteine; In diethyl ether; hexane; cyclohexane; at -78 ℃; for 4h;

cyclopropylboronic acid pinacol ester; In diethyl ether; hexane; cyclohexane; at -78 ℃; Reflux;
DOI:10.1021/ja2077813