O-(2,3,4-Tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide

Base Information

Chemical Name:O-(2,3,4-Tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide
CAS No.:87216-73-7
Molecular Formula:C₅₄H₅₇N₃O₁₀
Molecular Weight:908.061
Hs Code.:

Synonyms:O-(2,3,4-Tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide

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Chemical Property of O-(2,3,4-Tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide

Chemical Property:

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Technology Process of O-(2,3,4-Tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide

There total 10 articles about O-(2,3,4-Tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (2R,3R,4S,5R)-6-((2R,3R,4S,5R,6S)-6-azido-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-ylmethoxy)-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-ylmethyl ester

: 87216-73-7
O-(2,3,4-Tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide

: 87216-71-5
O-(2,3,4-Tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 2h; Yield given. Yields of byproduct given;

Reference yield:

: 82557-31-1
6-O-Trityl-α-D-glucopyranosyl azide

: 87216-73-7
O-(2,3,4-Tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide

Guidance literature:: Multi-step reaction with 4 steps

2: 65.9 percent / aq. AcOH, NaI

3: AgOSO₂CF₃, 1,1,3,3,-N,N'-tetramethylurea / 1,2-dichloro-ethane / 14 h / 20 °C

4: NaOMe / tetrahydrofuran; methanol / 2 h / 20 °C

With sodium methylate; silver trifluoromethanesulfonate; acetic acid; tetramethylurea; sodium iodide; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;

Reference yield:

: 87216-68-0
1-azido-2,3,4-tri-O-benzyl-α-D-glucopyranose

: 87216-73-7
O-(2,3,4-Tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: AgOSO₂CF₃, 1,1,3,3,-N,N'-tetramethylurea / 1,2-dichloro-ethane / 14 h / 20 °C

2: NaOMe / tetrahydrofuran; methanol / 2 h / 20 °C

With sodium methylate; silver trifluoromethanesulfonate; tetramethylurea; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;