6-<2-hydroxy-1-(isopropylthio)ethyl>-o-cresol

Base Information

• Chemical Name: 6-<2-hydroxy-1-(isopropylthio)ethyl>-o-cresol
• CAS No.: 121045-21-4
• Molecular Formula: C₁₂H₁₈O₂S
• Molecular Weight: 226.34

Synonyms:6-<2-hydroxy-1-(isopropylthio)ethyl>-o-cresol

Chemical Property of 6-<2-hydroxy-1-(isopropylthio)ethyl>-o-cresol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-<2-hydroxy-1-(isopropylthio)ethyl>-o-cresol

There total 3 articles about 6-<2-hydroxy-1-(isopropylthio)ethyl>-o-cresol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid 2-(2-hydroxy-3-methyl-phenyl)-2-isopropylsulfanyl-ethyl ester → 6-<2-hydroxy-1-(isopropylthio)ethyl>-o-cresol (121045-21-4)

Guidance literature:

With potassium carbonate; In methanol; water; for 20h; Yield given; Ambient temperature;

Reference yield:

2-(isopropylthio)ethyl acetate (5862-49-7) → 6-<2-hydroxy-1-(isopropylthio)ethyl>-o-cresol (121045-21-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) sulphuryl chloride; 2) triethylamine / 1) CH₂Cl₂, -40 deg C, 20 min; 2) CH₂Cl₂, -40 to 20 deg C

2: potassium carbonate / methanol; H₂O / 20 h / Ambient temperature

With sulfuryl dichloride; potassium carbonate; triethylamine; In methanol; water;

Reference yield:

ortho-cresol (95-48-7,77504-84-8) → 6-<2-hydroxy-1-(isopropylthio)ethyl>-o-cresol (121045-21-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) sulphuryl chloride; 2) triethylamine / 1) CH₂Cl₂, -40 deg C, 20 min; 2) CH₂Cl₂, -40 to 20 deg C

2: potassium carbonate / methanol; H₂O / 20 h / Ambient temperature

With sulfuryl dichloride; potassium carbonate; triethylamine; In methanol; water;

upstream raw materials:

2-(isopropylthio)ethyl acetate

ortho-cresol

Downstream raw materials:

7-methylbenzofuran

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