3,3-dichlorocyclobutanecarbonitrile

Base Information

Chemical Name:3,3-dichlorocyclobutanecarbonitrile
CAS No.:27744-70-3
Molecular Formula:C₅H₅Cl₂N
Molecular Weight:150.007
Hs Code.:

Synonyms:3,3-dichlorocyclobutanecarbonitrile

Suppliers and Price of 3,3-dichlorocyclobutanecarbonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-dichlorocyclobutanecarbonitrile

Chemical Property:

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Technology Process of 3,3-dichlorocyclobutanecarbonitrile

There total 2 articles about 3,3-dichlorocyclobutanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20249-16-5
3-oxo-cyclobutanecarbonitrile

: 27744-70-3
3,3-dichlorocyclobutanecarbonitrile

Guidance literature:: With phosphorus pentachloride; In tetrachloromethane;
DOI:10.1021/ja00730a021

Reference yield:

: 15760-35-7
3-methylenecyclobutanecarbonitrile

: 27744-70-3
3,3-dichlorocyclobutanecarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: NaIO₄, OsO₄ / H₂O; diethyl ether

2: PCl₅ / CCl₄

With sodium periodate; osmium(VIII) oxide; phosphorus pentachloride; In tetrachloromethane; diethyl ether; water;
DOI:10.1021/ja00730a021

Reference yield:

: 27744-70-3
3,3-dichlorocyclobutanecarbonitrile

: 23745-75-7
3-chlorobicyclobutane-1-carbonitrile

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 30.4 - 50.2 ℃; Thermodynamic data; Rate constant; 1,3-dehydrohalogenation, ΔH(excit.), ΔS(excit.);
DOI:10.1021/ja00258a038