C₄₈H₉₄O₉Si₃

Base Information

Chemical Name:C₄₈H₉₄O₉Si₃
CAS No.:908866-30-8
Molecular Formula:C₄₈H₉₄O₉Si₃
Molecular Weight:899.525
Hs Code.:

C<sub>48</sub>H<sub>94</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₄₈H₉₄O₉Si₃

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Chemical Property of C₄₈H₉₄O₉Si₃

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Technology Process of C₄₈H₉₄O₉Si₃

There total 1 articles about C₄₈H₉₄O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 908866-29-5
C₆₄H₁₁₂O₉Si₄

: C₄₂H₈₀O₉Si₂

: 908866-30-8
C₄₈H₉₄O₉Si₃

: 908866-46-6
C₅₈H₉₈O₉Si₃

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 13h;
DOI:10.1021/ja066772y

Reference yield:

: 908866-30-8
C₄₈H₉₄O₉Si₃

: 908866-36-4
C₆₇H₁₀₈O₈Si₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: Dess-Martin periodinane / CH₂Cl₂ / 0.75 h / 20 °C

2.1: K₂CO₃ / methanol / 17 h / 20 °C

3.1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 0.5 h / -78 °C

3.2: 42.8 mg / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 1 h / -78 - 20 °C

4.1: 96 percent / HF*pyridine / tetrahydrofuran / 1 h / 20 °C

5.1: 99 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

6.1: CuCN / tetrahydrofuran / 0.33 h / 0 °C

6.2: tetrahydrofuran / -78 - 0 °C

7.1: 62.0 mg / N-iodosuccinimide / tetrahydrofuran; acetonitrile / 5 h / 20 °C

8.1: 37.0 mg / Pd₂(dba)3; Ph₃As; copper(I) thiophene-2-carboxylate / tetrahydrofuran; dimethylsulfoxide / 2 h / 20 °C

9.1: 99 percent / imidazole / dimethylformamide / 1 h / 0 °C

10.1: 75 percent / PPTS / CH₂Cl₂; methanol / 1 h / 0 °C

11.1: SO₃*pyridine; Et₃N / CH₂Cl₂; dimethylsulfoxide / 5 h / 0 °C

12.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

12.2: 11.7 mg / tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C

13.1: 77 percent / aq. H₂O₂; NaHCO₃ / tetrahydrofuran / 9 h / 20 °C

With 1H-imidazole; N-iodo-succinimide; n-butyllithium; copper(I) thiophene-2-carboxylate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; pyridine-SO₃ complex; triphenyl-arsane; dihydrogen peroxide; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; 8.1: Stille coupling / 12.2: Wittig reaction;
DOI:10.1021/ja066772y

Reference yield:

: 908866-30-8
C₄₈H₉₄O₉Si₃

: C₆₄H₁₀₄O₉Si₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: Dess-Martin periodinane / CH₂Cl₂ / 0.75 h / 20 °C

2.1: K₂CO₃ / methanol / 17 h / 20 °C

3.1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 0.5 h / -78 °C

3.2: 42.8 mg / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 1 h / -78 - 20 °C

4.1: 96 percent / HF*pyridine / tetrahydrofuran / 1 h / 20 °C

5.1: 99 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

6.1: CuCN / tetrahydrofuran / 0.33 h / 0 °C

6.2: tetrahydrofuran / -78 - 0 °C

7.1: 62.0 mg / N-iodosuccinimide / tetrahydrofuran; acetonitrile / 5 h / 20 °C

8.1: 37.0 mg / Pd₂(dba)3; Ph₃As; copper(I) thiophene-2-carboxylate / tetrahydrofuran; dimethylsulfoxide / 2 h / 20 °C

9.1: 99 percent / imidazole / dimethylformamide / 1 h / 0 °C

10.1: 75 percent / PPTS / CH₂Cl₂; methanol / 1 h / 0 °C

11.1: SO₃*pyridine; Et₃N / CH₂Cl₂; dimethylsulfoxide / 5 h / 0 °C

With 1H-imidazole; N-iodo-succinimide; n-butyllithium; copper(I) thiophene-2-carboxylate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; pyridine-SO₃ complex; triphenyl-arsane; pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; 8.1: Stille coupling;
DOI:10.1021/ja066772y