benzyl 5-deoxy-2,3-O-isopropylidene-5-(1H-tetrazol-5-yl)-β-D-ribofuranoside

Base Information

Chemical Name:benzyl 5-deoxy-2,3-O-isopropylidene-5-(1H-tetrazol-5-yl)-β-D-ribofuranoside
CAS No.:1382059-90-6
Molecular Formula:C₁₆H₂₀N₄O₄
Molecular Weight:332.359
Hs Code.:

Synonyms:benzyl 5-deoxy-2,3-O-isopropylidene-5-(1H-tetrazol-5-yl)-β-D-ribofuranoside

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Chemical Property of benzyl 5-deoxy-2,3-O-isopropylidene-5-(1H-tetrazol-5-yl)-β-D-ribofuranoside

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Technology Process of benzyl 5-deoxy-2,3-O-isopropylidene-5-(1H-tetrazol-5-yl)-β-D-ribofuranoside

There total 3 articles about benzyl 5-deoxy-2,3-O-isopropylidene-5-(1H-tetrazol-5-yl)-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1382059-89-3
benzyl 5-cyano-5-deoxy-2,3-O-isopropylidene-β-D-ribofuranoside

: 1382059-90-6
benzyl 5-deoxy-2,3-O-isopropylidene-5-(1H-tetrazol-5-yl)-β-D-ribofuranoside

Guidance literature:: With trimethylsilylazide; di(n-butyl)tin oxide; In toluene; at 120 ℃; for 16h;
DOI:10.1021/ol3013638

Reference yield:

: 23276-32-6
benzyl 2,3-O-isopropylidene-D-ribofuranoside

: 1382059-90-6
benzyl 5-deoxy-2,3-O-isopropylidene-5-(1H-tetrazol-5-yl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 0.5 h / -20 °C / Inert atmosphere

2: potassium cyanide / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

3: trimethylsilylazide; di(n-butyl)tin oxide / toluene / 16 h / 120 °C

With pyridine; potassium cyanide; trimethylsilylazide; di(n-butyl)tin oxide; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol3013638

Reference yield:

: 70209-12-0
benzyl 2,3-O-isopropylidene-5-O-triflyl-β-D-ribofuranoside

: 1382059-90-6
benzyl 5-deoxy-2,3-O-isopropylidene-5-(1H-tetrazol-5-yl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: potassium cyanide / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

2: trimethylsilylazide; di(n-butyl)tin oxide / toluene / 16 h / 120 °C

With potassium cyanide; trimethylsilylazide; di(n-butyl)tin oxide; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol3013638