5-([1,3]dioxolo[4,5-g]quinolin-7-yl)-2,3-dimethoxyphenyl trifluoromethanesulfonate

Base Information

Chemical Name:5-([1,3]dioxolo[4,5-g]quinolin-7-yl)-2,3-dimethoxyphenyl trifluoromethanesulfonate
CAS No.:1353555-71-1
Molecular Formula:C₁₉H₁₄F₃NO₇S
Molecular Weight:457.384
Hs Code.:

Synonyms:5-([1,3]dioxolo[4,5-g]quinolin-7-yl)-2,3-dimethoxyphenyl trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-([1,3]dioxolo[4,5-g]quinolin-7-yl)-2,3-dimethoxyphenyl trifluoromethanesulfonate

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Technology Process of 5-([1,3]dioxolo[4,5-g]quinolin-7-yl)-2,3-dimethoxyphenyl trifluoromethanesulfonate

There total 2 articles about 5-([1,3]dioxolo[4,5-g]quinolin-7-yl)-2,3-dimethoxyphenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1353555-70-0
5-([1,3]dioxolo[4,5-g]quinolin-7-yl)-2,3-dimethoxyphenol

: 1353555-71-1
5-([1,3]dioxolo[4,5-g]quinolin-7-yl)-2,3-dimethoxyphenyl trifluoromethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;

Reference yield:

: 1353555-69-7
7-(3-(benzyloxy)-4,5-dimethoxyphenyl)-[1,3]-dioxolo[4,5-g]quinoline

: 1353555-71-1
5-([1,3]dioxolo[4,5-g]quinolin-7-yl)-2,3-dimethoxyphenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / 8 h / 60 °C / 760.05 Torr

2: triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

With hydrogen; triethylamine; palladium 10% on activated carbon; In dichloromethane;