C₂₀H₂₃NO₅

Base Information

Chemical Name:C₂₀H₂₃NO₅
CAS No.:1430812-33-1
Molecular Formula:C₂₀H₂₃NO₅
Molecular Weight:357.406
Hs Code.:

C<sub>20</sub>H<sub>23</sub>NO<sub>5</sub>

Synonyms:C₂₀H₂₃NO₅

Suppliers and Price of C₂₀H₂₃NO₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₀H₂₃NO₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₀H₂₃NO₅

There total 9 articles about C₂₀H₂₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1430812-31-9
C₂₀H₂₁BrO₅

: 1430812-33-1
C₂₀H₂₃NO₅

Guidance literature:: With copper(l) iodide; sodium azide; sodium L-ascorbate; N,N`-dimethylethylenediamine; In water; dimethyl sulfoxide; at 60 ℃; for 12h;
DOI:10.1016/j.ejmech.2012.12.042

Reference yield:

: 63638-85-7
3-bromo-2-hydroxy-4-methoxybenzaldehyde

: 1430812-33-1
C₂₀H₂₃NO₅

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / acetonitrile / 1 h / Reflux

2: tetrahydrofuran / 1 h / 0 - 20 °C

3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 1 h / 20 °C / Inert atmosphere

4: hydrogen; palladium on activated charcoal / acetic acid; methanol / 1 h / 20 °C

5: pyridinium chlorochromate / dichloromethane / 4 h

6: toluene-4-sulfonic acid; magnesium sulfate / 2 h / Reflux

7: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; lithium tert-butoxide / 1,4-dioxane / 1 h / 90 °C

8: N,N`-dimethylethylenediamine; copper(l) iodide; sodium azide; sodium L-ascorbate / water; dimethyl sulfoxide / 12 h / 60 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; sodium azide; palladium on activated charcoal; hydrogen; magnesium sulfate; potassium carbonate; toluene-4-sulfonic acid; sodium L-ascorbate; pyridinium chlorochromate; lithium tert-butoxide; N,N`-dimethylethylenediamine; XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetic acid; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.ejmech.2012.12.042

Reference yield:

: 1430812-47-7
9-bromo-8-methoxy-3,4-dihydrobenzo[b]oxepin-5(2H)-one

: 1430812-33-1
C₂₀H₂₃NO₅

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid; magnesium sulfate / 2 h / Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; lithium tert-butoxide / 1,4-dioxane / 1 h / 90 °C

3: N,N`-dimethylethylenediamine; copper(l) iodide; sodium azide; sodium L-ascorbate / water; dimethyl sulfoxide / 12 h / 60 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; sodium azide; magnesium sulfate; toluene-4-sulfonic acid; sodium L-ascorbate; lithium tert-butoxide; N,N`-dimethylethylenediamine; XPhos; In 1,4-dioxane; water; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2012.12.042