methyl 3-(2-acetylfuran-3-yl)-6-(benzenesulfonylmethyl)-2-hydroxybenzoate

Base Information

Chemical Name:methyl 3-(2-acetylfuran-3-yl)-6-(benzenesulfonylmethyl)-2-hydroxybenzoate
CAS No.:1356112-33-8
Molecular Formula:C₂₁H₁₈O₇S
Molecular Weight:414.436
Hs Code.:

Synonyms:methyl 3-(2-acetylfuran-3-yl)-6-(benzenesulfonylmethyl)-2-hydroxybenzoate

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Chemical Property of methyl 3-(2-acetylfuran-3-yl)-6-(benzenesulfonylmethyl)-2-hydroxybenzoate

Chemical Property:

Purity/Quality:

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Technology Process of methyl 3-(2-acetylfuran-3-yl)-6-(benzenesulfonylmethyl)-2-hydroxybenzoate

There total 6 articles about methyl 3-(2-acetylfuran-3-yl)-6-(benzenesulfonylmethyl)-2-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49777-66-4
1-(3-dihydroxyboranyl-furan-2-yl)-ethanone

: 1286180-37-7
methyl 6-(benzenesulphonylmethyl)-3-bromo-2-hydroxybenzoate

: 1356112-33-8
methyl 3-(2-acetylfuran-3-yl)-6-(benzenesulfonylmethyl)-2-hydroxybenzoate

Guidance literature:: With potassium fluoride monohydrate; sodium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In sulfuryl dichloride;

Reference yield:

: 873-55-2
sodium benzenesulfonate

: 1356112-33-8
methyl 3-(2-acetylfuran-3-yl)-6-(benzenesulfonylmethyl)-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / water; N,N-dimethyl acetamide / 2 h / 90 °C

2: aluminum (III) chloride; N,N-dimethyl-aniline / dichloromethane / 0.83 h

3: sodium iodide; potassium fluoride monohydrate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / sulfuryl dichloride

With aluminum (III) chloride; potassium fluoride monohydrate; sodium hydrogencarbonate; N,N-dimethyl-aniline; sodium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In sulfuryl dichloride; dichloromethane; N,N-dimethyl acetamide; water;

Reference yield:

: 1286179-58-5
methyl 6-(benzenesulphonylmethyl)-3-bromo-2-methoxybenzoate

: 1356112-33-8
methyl 3-(2-acetylfuran-3-yl)-6-(benzenesulfonylmethyl)-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride; N,N-dimethyl-aniline / dichloromethane / 0.83 h

2: sodium iodide; potassium fluoride monohydrate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / sulfuryl dichloride

With aluminum (III) chloride; potassium fluoride monohydrate; N,N-dimethyl-aniline; sodium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In sulfuryl dichloride; dichloromethane;