(Z)-2-carbomethoxyethenyl o-bromophenyl sulfoxide

Base Information

• Chemical Name: (Z)-2-carbomethoxyethenyl o-bromophenyl sulfoxide
• CAS No.: 1315563-25-7
• Molecular Formula: C₁₀H₉BrO₃S
• Molecular Weight: 289.15

Synonyms:(Z)-2-carbomethoxyethenyl o-bromophenyl sulfoxide

Chemical Property of (Z)-2-carbomethoxyethenyl o-bromophenyl sulfoxide

Chemical Property:

Purity/Quality:

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Technology Process of (Z)-2-carbomethoxyethenyl o-bromophenyl sulfoxide

There total 3 articles about (Z)-2-carbomethoxyethenyl o-bromophenyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

methyl (Z)-3-((2-bromophenyl)thio)acrylate → (Z)-2-carbomethoxyethenyl o-bromophenyl sulfoxide (1315563-25-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 20 ℃; Schlenk technique;

DOI:10.1021/acs.orglett.6b03827

Reference yield:

C10H9BrO2S → (Z)-2-carbomethoxyethenyl o-bromophenyl sulfoxide (1315563-25-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃;

DOI:10.1021/ol201508e

Reference yield:

o-bromothiophenol (6320-02-1) → (Z)-2-carbomethoxyethenyl o-bromophenyl sulfoxide (1315563-25-7)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/ol201508e

upstream raw materials:

o-bromothiophenol

Downstream raw materials:

C₂₀H₂₄BrNO₃S

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