(+)-(7S)-sydonic acid

Base Information

Chemical Name:(+)-(7S)-sydonic acid
CAS No.:1137089-32-7
Molecular Formula:C₁₅H₂₂O₄
Molecular Weight:266.337
Hs Code.:

Synonyms:(+)-(7S)-sydonic acid

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Chemical Property of (+)-(7S)-sydonic acid

Chemical Property:

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Technology Process of (+)-(7S)-sydonic acid

There total 12 articles about (+)-(7S)-sydonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1461710-43-9
C₂₃H₄₀O₄Si

: 1137089-32-7
(+)-(7S)-sydonic acid

Guidance literature:: C₂₃H₄₀O₄Si; With sodium hydroxide; In methanol; for 0.5h; Reflux;

With hydrogenchloride; In methanol; water; at 0 ℃;
DOI:10.1016/j.tetasy.2013.07.011

Reference yield:

: 108005-72-7
((2S,3S)-3-methyl-3-(4-methylpentyl)oxiran-2-yl)methanol

: 1137089-32-7
(+)-(7S)-sydonic acid

Guidance literature:: Multi-step reaction with 10 steps

1.1: triphenylphosphine; sodium hydrogencarbonate; tetrachloromethane / 5 h / Reflux

2.1: tetrahydrofuran; hexane / -78 - 20 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether; toluene / 1.5 h / 0 - 20 °C / Inert atmosphere

4.1: pyridine / 2 h / 20 °C

5.1: 1H-imidazole; dmap / tetrahydrofuran / 3 h / 60 °C / Inert atmosphere

6.1: sodium hydroxide / methanol / 0.5 h / 20 °C

7.1: manganese(IV) oxide / dichloromethane / 4 h / Reflux

8.1: BHA / toluene / 3 h / 80 °C / Inert atmosphere

9.1: trifluoroacetic anhydride; triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

10.1: sodium hydroxide / methanol / 0.5 h / Reflux

10.2: 0 °C

With pyridine; 1H-imidazole; tetrachloromethane; dmap; manganese(IV) oxide; sodium hydrogencarbonate; triethylamine; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; trifluoroacetic anhydride; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; toluene;
DOI:10.1016/j.tetasy.2013.07.011

Reference yield:

: 1461710-37-1
(S,E)-4,8-dimethylnon-2-ene-1,4-diol

: 1137089-32-7
(+)-(7S)-sydonic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / 2 h / 20 °C

2.1: 1H-imidazole; dmap / tetrahydrofuran / 3 h / 60 °C / Inert atmosphere

3.1: sodium hydroxide / methanol / 0.5 h / 20 °C

4.1: manganese(IV) oxide / dichloromethane / 4 h / Reflux

5.1: BHA / toluene / 3 h / 80 °C / Inert atmosphere

6.1: trifluoroacetic anhydride; triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

7.1: sodium hydroxide / methanol / 0.5 h / Reflux

7.2: 0 °C

With pyridine; 1H-imidazole; dmap; manganese(IV) oxide; triethylamine; trifluoroacetic anhydride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tetasy.2013.07.011