1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-sn-glycero-3-phosphocholine

Base Information

Chemical Name:1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-sn-glycero-3-phosphocholine
CAS No.:685888-07-7
Molecular Formula:C₃₃H₅₀NO₇P
Molecular Weight:603.736
Hs Code.:

Synonyms:1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-sn-glycero-3-phosphocholine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-sn-glycero-3-phosphocholine

Chemical Property:

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Technology Process of 1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-sn-glycero-3-phosphocholine

There total 17 articles about 1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-sn-glycero-3-phosphocholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 685888-12-4
1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-2-O-(4-methoxybenzyl)-sn-glycero-3-phosphocholine

: 685888-07-7
1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-sn-glycero-3-phosphocholine

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃;

Reference yield:

: 108-88-3,15644-74-3,16713-13-6
toluene

: 685888-07-7
1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-sn-glycero-3-phosphocholine

Guidance literature:: Multi-step reaction with 9 steps

1.1: 89 percent / AlCl₃ / 3 h / Heating

2.1: 9-BBN / tetrahydrofuran / 5 h / 0 - 20 °C

2.2: 63 percent / Cs₂CO₃; AsPh₃; Pd(dppf)Cl₂*CH₂Cl₂ / tetrahydrofuran; dimethylformamide; H₂O / 20 - 75 °C

3.1: 94 percent / aq. K₂CO₃ / methanol

4.1: 81 percent / BF₃*OEt₂ / CHCl₃ / 48 h / 20 °C

5.1: 100 percent / CF₃SO₃H / diethyl ether / 0.33 h / 0 °C

6.1: 78 percent / dimethylsulfoxide; dimethylformamide / 72 h

7.1: 100 percent / K₂CO₃ / methanol

8.1: POCl₃; Et₃N / CHCl₃ / -10 - 20 °C

8.2: 84 percent / pyridine / CHCl₃ / 48 h / 20 °C

9.1: 65 percent / aq. DDQ / CH₂Cl₂ / 20 °C

With 9-borabicyclo[3.3.1]nonane dimer; aluminium trichloride; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; potassium carbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; 1.1: Friedel-Crafts reaction;

Reference yield:

: 821-41-0
5-Hexen-1-ol

: 685888-07-7
1-O-{11-[4-(4-methylbenzoyl)phenyl]-5-undecenyl}-sn-glycero-3-phosphocholine

Guidance literature:: Multi-step reaction with 11 steps

1.1: 67 percent / PPh₃; imidazole; I₂ / CH₂Cl₂ / 2 h / 20 °C

2.1: 91 percent / nitromethane / Heating

3.1: n-BuLi / diethyl ether / 1 h / 20 °C

3.2: 56 percent / diethyl ether / -78 - 20 °C

4.1: 9-BBN / tetrahydrofuran / 5 h / 0 - 20 °C

4.2: 63 percent / Cs₂CO₃; AsPh₃; Pd(dppf)Cl₂*CH₂Cl₂ / tetrahydrofuran; dimethylformamide; H₂O / 20 - 75 °C

5.1: 94 percent / aq. K₂CO₃ / methanol

6.1: 81 percent / BF₃*OEt₂ / CHCl₃ / 48 h / 20 °C

7.1: 100 percent / CF₃SO₃H / diethyl ether / 0.33 h / 0 °C

8.1: 78 percent / dimethylsulfoxide; dimethylformamide / 72 h

9.1: 100 percent / K₂CO₃ / methanol

10.1: POCl₃; Et₃N / CHCl₃ / -10 - 20 °C

10.2: 84 percent / pyridine / CHCl₃ / 48 h / 20 °C

11.1: 65 percent / aq. DDQ / CH₂Cl₂ / 20 °C

With 1H-imidazole; 9-borabicyclo[3.3.1]nonane dimer; n-butyllithium; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; iodine; potassium carbonate; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; In tetrahydrofuran; methanol; diethyl ether; nitromethane; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;