C₂₁H₃₀O₆

Base Information

• Chemical Name: C₂₁H₃₀O₆
• CAS No.: 950190-86-0
• Molecular Formula: C₂₁H₃₀O₆
• Molecular Weight: 378.466
• Mol file: 950190-86-0.mol

Synonyms:C₂₁H₃₀O₆

Chemical Property of C₂₁H₃₀O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₁H₃₀O₆

There total 6 articles about C₂₁H₃₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C24H36O7 → C21H30O6 (950190-86-0)

Guidance literature:

With perchloric acid; In dichloromethane; water; at 20 ℃; for 36h;

DOI:10.1021/ol071282b

Reference yield:

C13H24O3S2 (950190-83-7) → C21H30O6 (950190-86-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: potassium tert-butoxide; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: tetrahydrofuran; hexane / 2 h / -78 °C

1.3: 77 percent / tetrahydrofuran; hexane / 0.83 h / -78 - 0 °C

2.1: 75 percent / calcium carbonate; mercury(II) perchlorate trihydrate / tetrahydrofuran; H₂O / 0.08 h / 0 °C

3.1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 96 h / -35 °C

4.1: p-toluenesulfonic acid monohydrate / acetone / 0.13 h / 20 °C

5.1: 2.0 g / perchloric acid / CH₂Cl₂; H₂O / 36 h / 20 °C

With n-butyllithium; perchloric acid; mercury(II) perchlorate; potassium tert-butylate; toluene-4-sulfonic acid; acetic acid; calcium carbonate; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; hexane; dichloromethane; water; acetone; acetonitrile;

DOI:10.1021/ol071282b

Reference yield:

C30H50O8Si (950190-80-4) → C21H30O6 (950190-86-0)

Guidance literature:

Multi-step reaction with 3 steps

1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 96 h / -35 °C

2: p-toluenesulfonic acid monohydrate / acetone / 0.13 h / 20 °C

3: 2.0 g / perchloric acid / CH₂Cl₂; H₂O / 36 h / 20 °C

With perchloric acid; toluene-4-sulfonic acid; acetic acid; tetramethylammonium triacetoxyborohydride; In dichloromethane; water; acetone; acetonitrile;

DOI:10.1021/ol071282b

upstream raw materials:

C₁₃H₂₄O₃S₂

C₃₆H₆₂O₆S₄Si

C₃₀H₅₀O₈Si

Downstream raw materials:

C₃₇H₄₈O₆Si

C₄₄H₅₄O₆Si

C₄₄H₅₄O₇Si

C₃₁H₄₄O₆Si