Technology Process of C23H23F2NO2
There total 5 articles about C23H23F2NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium hexamethyldisilazane;
In
tetrahydrofuran; toluene;
at 100 ℃;
for 5h;
Inert atmosphere;
Sealed tube;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / dichloromethane / 0.25 h / 20 °C
1.2: 20 °C
2.1: sodium fluoride / 100 °C / Neat (no solvent)
3.1: potassium hydroxide; water / methanol / 20 °C
4.1: pyridine / dichloromethane / 20 °C
5.1: lithium hexamethyldisilazane / toluene; tetrahydrofuran / 5 h / 100 °C / Inert atmosphere; Sealed tube; Microwave irradiation
With
water; sodium fluoride; triethylamine; potassium hydroxide; lithium hexamethyldisilazane;
pyridine;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide; water / methanol / 20 °C
2: pyridine / dichloromethane / 20 °C
3: lithium hexamethyldisilazane / toluene; tetrahydrofuran / 5 h / 100 °C / Inert atmosphere; Sealed tube; Microwave irradiation
With
water; potassium hydroxide; lithium hexamethyldisilazane;
pyridine;
In
tetrahydrofuran; methanol; dichloromethane; toluene;