benzyl 2-azido-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside

Base Information

Chemical Name:benzyl 2-azido-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside
CAS No.:639460-01-8
Molecular Formula:C₂₆H₃₃N₃O₁₄
Molecular Weight:611.56
Hs Code.:

Synonyms:benzyl 2-azido-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside

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Chemical Property of benzyl 2-azido-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside

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Technology Process of benzyl 2-azido-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside

There total 3 articles about benzyl 2-azido-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 581814-26-8
benzyl 2-azido-4,6-benzylidene-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside

: 639460-01-8
benzyl 2-azido-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside

Guidance literature:: With acetic acid; at 80 ℃; for 1h;
DOI:10.1021/ja036584x

Reference yield:

: 92420-89-8
methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: 639460-01-8
benzyl 2-azido-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / trimethylsilyl trifluoromethanesulfonate; MS₄A / CH₂Cl₂ / 1 h

2: 93 percent / aq. acetic acid / 1 h / 80 °C

With trimethylsilyl trifluoromethanesulfonate; acetic acid; In dichloromethane;
DOI:10.1021/ja036584x

Reference yield:

: 103833-25-6
Benzyl-2-azido-4,6-O-benzyliden-2-desoxy-β-D-galactopyranosid

: 639460-01-8
benzyl 2-azido-2-deoxy-3-O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / trimethylsilyl trifluoromethanesulfonate; MS₄A / CH₂Cl₂ / 1 h

2: 93 percent / aq. acetic acid / 1 h / 80 °C

With trimethylsilyl trifluoromethanesulfonate; acetic acid; In dichloromethane;
DOI:10.1021/ja036584x