[16-(4'-Heptyl-biphenyl-4-carbonyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(4'-heptyl-biphenyl-4-yl)-methanone

Base Information

• Chemical Name: [16-(4'-Heptyl-biphenyl-4-carbonyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(4'-heptyl-biphenyl-4-yl)-methanone
• CAS No.: 124513-32-2
• Molecular Formula: C₅₂H₇₀N₂O₆
• Molecular Weight: 819.138

Synonyms:[16-(4'-Heptyl-biphenyl-4-carbonyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(4'-heptyl-biphenyl-4-yl)-methanone

Chemical Property of [16-(4'-Heptyl-biphenyl-4-carbonyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(4'-heptyl-biphenyl-4-yl)-methanone

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Technology Process of [16-(4'-Heptyl-biphenyl-4-carbonyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(4'-heptyl-biphenyl-4-yl)-methanone

There total 2 articles about [16-(4'-Heptyl-biphenyl-4-carbonyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(4'-heptyl-biphenyl-4-yl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

4'-heptylbiphenyl-4-ylcarboxylic acid chloride (58573-87-8) + 1,4,10,13-tetraoxa-7,16-diazacyclooctadecane (23978-55-4) → [16-(4'-Heptyl-biphenyl-4-carbonyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(4'-heptyl-biphenyl-4-yl)-methanone (124513-32-2)

Guidance literature:

With triethylamine; In dichloromethane; for 5h; Heating;

DOI:10.1021/jo00289a028

Reference yield:

4-(4-heptylphenyl)benzoic acid (58573-94-7) → [16-(4'-Heptyl-biphenyl-4-carbonyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(4'-heptyl-biphenyl-4-yl)-methanone (124513-32-2)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂

2: 76 percent / Et₃N / CH₂Cl₂ / 5 h / Heating

With thionyl chloride; triethylamine; In dichloromethane;

DOI:10.1021/jo00289a028

Reference yield: 70.0%

[16-(4'-Heptyl-biphenyl-4-carbonyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(4'-heptyl-biphenyl-4-yl)-methanone (124513-32-2) → 7,16-Bis-(4'-heptyl-biphenyl-4-ylmethyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane (124513-34-4)

Guidance literature:

With diborane; In tetrahydrofuran;

DOI:10.1021/jo00289a028

upstream raw materials:

4'-heptylbiphenyl-4-ylcarboxylic acid chloride

1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

4-(4-heptylphenyl)benzoic acid

Downstream raw materials:

7,16-Bis-(4'-heptyl-biphenyl-4-ylmethyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

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