Diethyl-carbamic acid 1-methylene-3-phenyl-3-triisopropylsilanyloxy-propyl ester

Base Information

Chemical Name:Diethyl-carbamic acid 1-methylene-3-phenyl-3-triisopropylsilanyloxy-propyl ester
CAS No.:147047-83-4
Molecular Formula:C₂₄H₄₁NO₃Si
Molecular Weight:419.68
Hs Code.:

Synonyms:Diethyl-carbamic acid 1-methylene-3-phenyl-3-triisopropylsilanyloxy-propyl ester

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Chemical Property of Diethyl-carbamic acid 1-methylene-3-phenyl-3-triisopropylsilanyloxy-propyl ester

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Technology Process of Diethyl-carbamic acid 1-methylene-3-phenyl-3-triisopropylsilanyloxy-propyl ester

There total 4 articles about Diethyl-carbamic acid 1-methylene-3-phenyl-3-triisopropylsilanyloxy-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 147047-81-2
Diethyl-carbamic acid 3-hydroxy-1-methylene-3-phenyl-propyl ester

: 147047-83-4
Diethyl-carbamic acid 1-methylene-3-phenyl-3-triisopropylsilanyloxy-propyl ester

Guidance literature:: With 2,6-dimethylpyridine;
DOI:10.1016/0040-4039(93)85089-F

Reference yield:

: 57933-92-3
<(diethylcarbamoyl)oxy>ethylene

: 147047-83-4
Diethyl-carbamic acid 1-methylene-3-phenyl-3-triisopropylsilanyloxy-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) sec-BuLi / 1) THF, -78 deg C

2: 81 percent / trimethylsilyl iodide

3: 97 percent / 2,6-lutidine

With 2,6-dimethylpyridine; trimethylsilyl iodide; sec.-butyllithium;
DOI:10.1016/0040-4039(93)85089-F

Reference yield:

: 147047-80-1
Diethyl-carbamic acid 1-bromo-vinyl ester

: 147047-83-4
Diethyl-carbamic acid 1-methylene-3-phenyl-3-triisopropylsilanyloxy-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / Ni(acac)2 / tetrahydrofuran

2: 81 percent / trimethylsilyl iodide

3: 97 percent / 2,6-lutidine

With 2,6-dimethylpyridine; trimethylsilyl iodide; bis(acetylacetonate)nickel(II); In tetrahydrofuran;
DOI:10.1016/0040-4039(93)85089-F