ethyl 2-methoxy>ethyl>-N-cyanoamino>acetate

Base Information

• Chemical Name: ethyl 2-methoxy>ethyl>-N-cyanoamino>acetate
• CAS No.: 97290-19-2
• Molecular Formula: C₂₅H₂₉Cl₂N₃O₇
• Molecular Weight: 554.427

Synonyms:ethyl 2-methoxy>ethyl>-N-cyanoamino>acetate

Chemical Property of ethyl 2-methoxy>ethyl>-N-cyanoamino>acetate

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Technology Process of ethyl 2-methoxy>ethyl>-N-cyanoamino>acetate

There total 2 articles about ethyl 2-methoxy>ethyl>-N-cyanoamino>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

bromocyane (506-68-3) + ethyl 2-<<2-<<4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>amino>acetate (97289-98-0) → ethyl 2-methoxy>ethyl>-N-cyanoamino>acetate (97290-19-2)

Guidance literature:

With sodium hydrogencarbonate; In chloroform; for 7.5h; Ambient temperature;

DOI:10.1021/jm00168a041

Reference yield:

2-[(2-aminoethoxy)methyl]-4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine (88150-50-9) → ethyl 2-methoxy>ethyl>-N-cyanoamino>acetate (97290-19-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 57 percent / K₂CO₃ / acetonitrile / 3.5 h / Heating

2: 62 percent / NaHCO₃ / CHCl₃ / 7.5 h / Ambient temperature

With sodium hydrogencarbonate; potassium carbonate; In chloroform; acetonitrile;

DOI:10.1021/jm00168a041

Reference yield: 69.0%

ethyl 2-methoxy>ethyl>-N-cyanoamino>acetate (97290-19-2) → 2-[2-(2-Amino-4-oxo-4,5-dihydro-imidazol-1-yl)-ethoxymethyl]-4-(2,3-dichloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester (97290-20-5)

Guidance literature:

With ammonium hydroxide; In methanol; for 16h; Ambient temperature;

DOI:10.1021/jm00168a041

upstream raw materials:

bromocyane

ethyl 2-<<2-<<4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyrid-2-yl>methoxy>ethyl>amino>acetate

2-[(2-aminoethoxy)methyl]-4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

Downstream raw materials:

2-[2-(2-Amino-4-oxo-4,5-dihydro-imidazol-1-yl)-ethoxymethyl]-4-(2,3-dichloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester

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