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Technology Process of Fe(C5H5)(C5H4)(CH)N(CH2)C5H4N(C6H4)C(CH3)3(1+)*B(C6H5)4(1-)=[Fe(C10H9)(CH)N(CH2)C5H4N(C6H4)C(CH3)3][B(C6H5)4]

Fe(C5H5)(C5H4)(CH)N(CH2)C5H4N(C6H4)C(CH3)3(1+)*B(C6H5)4(1-)=[Fe(C10H9)(CH)N(CH2)C5H4N(C6H4)C(CH3)3][B(C6H5)4]

Base Information
  • Chemical Name:Fe(C5H5)(C5H4)(CH)N(CH2)C5H4N(C6H4)C(CH3)3(1+)*B(C6H5)4(1-)=[Fe(C10H9)(CH)N(CH2)C5H4N(C6H4)C(CH3)3][B(C6H5)4]
  • CAS No.:250701-08-7
  • Molecular Formula:C24H20B*C27H29FeN2
  • Molecular Weight:756.621
  • Hs Code.:
Fe(C<sub>5</sub>H<sub>5</sub>)(C<sub>5</sub>H<sub>4</sub>)(CH)N(CH<sub>2</sub>)C<sub>5</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>4</sub>)C(CH<sub>3</sub>)3<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=[Fe(C<sub>10</sub>H<sub>9</sub>)(CH)N(CH<sub>2</sub>)C<sub>5</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>4</sub>)C(CH<sub>3</sub>)3][B(C<sub>6</sub>H<sub>5</sub>)4]

Synonyms:Fe(C5H5)(C5H4)(CH)N(CH2)C5H4N(C6H4)C(CH3)3(1+)*B(C6H5)4(1-)=[Fe(C10H9)(CH)N(CH2)C5H4N(C6H4)C(CH3)3][B(C6H5)4]

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Chemical Property of Fe(C5H5)(C5H4)(CH)N(CH2)C5H4N(C6H4)C(CH3)3(1+)*B(C6H5)4(1-)=[Fe(C10H9)(CH)N(CH2)C5H4N(C6H4)C(CH3)3][B(C6H5)4]
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Technology Process of Fe(C5H5)(C5H4)(CH)N(CH2)C5H4N(C6H4)C(CH3)3(1+)*B(C6H5)4(1-)=[Fe(C10H9)(CH)N(CH2)C5H4N(C6H4)C(CH3)3][B(C6H5)4]

There total 1 articles about Fe(C5H5)(C5H4)(CH)N(CH2)C5H4N(C6H4)C(CH3)3(1+)*B(C6H5)4(1-)=[Fe(C10H9)(CH)N(CH2)C5H4N(C6H4)C(CH3)3][B(C6H5)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

Fe(C<sub>5</sub>H<sub>5</sub>)(C<sub>5</sub>H<sub>4</sub>)CHC<sub>5</sub>H<sub>4</sub>N<sub>2</sub>

Fe(C5H5)(C5H4)CHC5H4N2

1-bromo-4-tert-butylbenzene
3972-65-4

1-bromo-4-tert-butylbenzene

sodium tetraphenyl borate
143-66-8

sodium tetraphenyl borate

Fe(C<sub>5</sub>H<sub>5</sub>)(C<sub>5</sub>H<sub>4</sub>)(CH)N(CH<sub>2</sub>)C<sub>5</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>4</sub>)C(CH<sub>3</sub>)3<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=[Fe(C<sub>10</sub>H<sub>9</sub>)(CH)N(CH<sub>2</sub>)C<sub>5</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>4</sub>)C(CH<sub>3</sub>)3][B(C<sub>6</sub>H<sub>5</sub>)4]
250701-08-7

Fe(C5H5)(C5H4)(CH)N(CH2)C5H4N(C6H4)C(CH3)3(1+)*B(C6H5)4(1-)=[Fe(C10H9)(CH)N(CH2)C5H4N(C6H4)C(CH3)3][B(C6H5)4]

Guidance literature:
In N,N-dimethyl-formamide; 80°C, 15 min, cooling, pptn. (Et2O/hexanes 1:1), filtration, washing (Et2O), dissoln. (acetone), stirring with NaBPh4 (12 h), acetone removal (vac.); extraction (CH2Cl2), crystn.; elem. anal.;
DOI:10.1021/ja9818607
upstream raw materials:

1-bromo-4-tert-butylbenzene

sodium tetraphenyl borate

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