Technology Process of C25H25(2)HO3
There total 9 articles about C25H25(2)HO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
toluene;
at 110 ℃;
Yield given;
DOI:10.1021/ja00074a046
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine
2: 47 percent / pyridine
3: 91 percent / NaOMe / methanol
4: 9 percent / LiAlD4 / tetrahydrofuran
5: DMAP / acetonitrile
6: Bu3SnH, AIBN / toluene / 110 °C
With
pyridine; dmap; lithium aluminium deuteride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate;
In
tetrahydrofuran; methanol; toluene; acetonitrile;
DOI:10.1021/ja00074a046
- Guidance literature:
-
Multi-step reaction with 7 steps
1: aq. NaOH
2: pyridine
3: 47 percent / pyridine
4: 91 percent / NaOMe / methanol
5: 9 percent / LiAlD4 / tetrahydrofuran
6: DMAP / acetonitrile
7: Bu3SnH, AIBN / toluene / 110 °C
With
pyridine; dmap; sodium hydroxide; lithium aluminium deuteride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate;
In
tetrahydrofuran; methanol; toluene; acetonitrile;
DOI:10.1021/ja00074a046