C₂₉H₃₁NO₇

Base Information

Chemical Name:C₂₉H₃₁NO₇
CAS No.:1026430-54-5
Molecular Formula:C₂₉H₃₁NO₇
Molecular Weight:505.568
Hs Code.:

C<sub>29</sub>H<sub>31</sub>NO<sub>7</sub>

Synonyms:C₂₉H₃₁NO₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₁NO₇

Chemical Property:

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Technology Process of C₂₉H₃₁NO₇

There total 1 articles about C₂₉H₃₁NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86827-18-1,92455-53-3,16677-29-5
N-benzyloxycarbonyl-O-benzyl-L-tyrosine

: 543-27-1
isobutyl chloroformate

: 1026430-54-5
C₂₉H₃₁NO₇

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide;

Reference yield:

: 1026430-54-5
C₂₉H₃₁NO₇

: 58822-25-6
Leu-enkephalin

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / dimethylformamide / 6 h

2: 79 percent / H₂ / Pd / acetic acid; methanol / 20 h

With hydrogen; palladium; In methanol; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 1026430-54-5
C₂₉H₃₁NO₇

: {(S)-3-tert-Butoxycarbonylamino-2-hydroxy-4-[4-(2-hydroxy-ethoxy)-phenyl]-butyl}-((S)-3-tert-butoxycarbonylamino-2-hydroxy-4-phenyl-butyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 13 steps

1: tetrahydrofuran; diethyl ether / 0 °C

2: HCl / dioxane / 0 °C

3: NaBH₄

4: KOH / ethanol

5: methanol / 50 °C

6: 92 percent / (i-Pr)2NEt / dimethylformamide / 2 h / 0 °C

7: H₂, 20percent Pd(OH)2/C / ethanol

8: Et₃N / methanol / 4 h

9: 98 percent / p-TsOH / benzene / 3 h / Heating

10: 86 percent / diethyl azodicarboxylate, Ph₃P / tetrahydrofuran / Ambient temperature

11: 98percent HCOOH / 0.33 h / 5 °C

12: Et₃N / methanol

13: H₂, 20percent Pd(OH)2/C / 20percent Pd(OH)2/C / methanol

With hydrogenchloride; palladium dihydroxide; potassium hydroxide; sodium tetrahydroborate; formic acid; hydrogen; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; palladium dihydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm950717a