C₆₈H₆₆O₂

Base Information

Chemical Name:C₆₈H₆₆O₂
CAS No.:1388114-04-2
Molecular Formula:C₆₈H₆₆O₂
Molecular Weight:915.271
Hs Code.:

C<sub>68</sub>H<sub>66</sub>O<sub>2</sub>

Synonyms:C₆₈H₆₆O₂

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Chemical Property of C₆₈H₆₆O₂

Chemical Property:

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Technology Process of C₆₈H₆₆O₂

There total 8 articles about C₆₈H₆₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1388114-03-1
C₃₄H₃₃BrO

: C₄₀H₄₅BO₃

: 1388114-04-2
C₆₈H₆₆O₂

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 80 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol3017353

Reference yield:

: 468751-38-4
ortho-(phenylsulfonylmethyl)benzaldehyde

: 1388114-04-2
C₆₈H₆₆O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethyl chlorophosphate; lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere

1.2: 2 h / -78 °C / Inert atmosphere

2.1: iodine(I) bromide / dichloromethane / 2 h / -78 °C / Inert atmosphere

3.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine / toluene / 35 °C / Inert atmosphere

4.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 2 h / 80 °C / Inert atmosphere

With potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; iodine(I) bromide; diethyl chlorophosphate; diisopropylamine; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; 3.1: Sonogashira coupling / 4.1: Suzuki coupling;
DOI:10.1021/ol3017353

Reference yield:

: 1337927-36-2
((4-((3,7-dimethyloctyl)oxy)phenyl)ethynyl)trimethylsilane

: 1388114-04-2
C₆₈H₆₆O₂

Guidance literature:: Multi-step reaction with 3 steps

1: water; potassium carbonate / tetrahydrofuran; methanol / 2 h / 20 °C / Inert atmosphere

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine / toluene / 35 °C / Inert atmosphere

3: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 2 h / 80 °C / Inert atmosphere

With potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; potassium carbonate; diisopropylamine; In tetrahydrofuran; 1,4-dioxane; methanol; water; toluene; 2: Sonogashira coupling / 3: Suzuki coupling;
DOI:10.1021/ol3017353