C₁₇H₁₇BrN₂O₂

Base Information

Chemical Name:C₁₇H₁₇BrN₂O₂
CAS No.:1049634-20-9
Molecular Formula:C₁₇H₁₇BrN₂O₂
Molecular Weight:361.238
Hs Code.:

C<sub>17</sub>H<sub>17</sub>BrN<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₇H₁₇BrN₂O₂

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Chemical Property of C₁₇H₁₇BrN₂O₂

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Technology Process of C₁₇H₁₇BrN₂O₂

There total 8 articles about C₁₇H₁₇BrN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 588-46-5
N-(phenylmethyl)acetamide

: 1049634-19-6
C₈H₈BrNO₂

: 1049634-20-9
C₁₇H₁₇BrN₂O₂

Guidance literature:: N-(phenylmethyl)acetamide; With 2,6-dimethylpyridine; oxalyl dichloride; In dichloromethane; at 0 ℃; for 0.5h;

C₈H₈BrNO₂; In dichloromethane; at 0 - 20 ℃; for 2.5h;

Reference yield:

: 6602-32-0
2-bromo-pyridin-3-ol

: 1049634-20-9
C₁₇H₁₇BrN₂O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Heating / reflux

2.1: tetraethylammonium chloride; potassium acetate / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 105 °C

3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide; tert-butyl alcohol / dichloromethane / 20 °C

4.1: sodium periodate / tetrahydrofuran; water / 2.5 h / 20 °C

5.1: sodium tetrahydroborate / methanol / 20 °C

5.2: 0.5 h

6.1: phosphorus tribromide / chloroform / 3.5 h / Heating / reflux

6.2: 0 °C

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

8.1: 2,6-dimethylpyridine; oxalyl dichloride / dichloromethane / 0.5 h / 0 °C

8.2: 2.5 h / 0 - 20 °C

With 2,6-dimethylpyridine; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; oxalyl dichloride; di-isopropyl azodicarboxylate; tetraethylammonium chloride; potassium acetate; phosphorus tribromide; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; tert-butyl alcohol; palladium diacetate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; 1.1: Mitsunobu reaction / 2.1: Intramolecular Heck cyclization;

Reference yield:

: 405174-45-0
2-bromo-3-(but-3-en-1-yloxy)pyridine

: 1049634-20-9
C₁₇H₁₇BrN₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetraethylammonium chloride; potassium acetate / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 105 °C

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide; tert-butyl alcohol / dichloromethane / 20 °C

3.1: sodium periodate / tetrahydrofuran; water / 2.5 h / 20 °C

4.1: sodium tetrahydroborate / methanol / 20 °C

4.2: 0.5 h

5.1: phosphorus tribromide / chloroform / 3.5 h / Heating / reflux

5.2: 0 °C

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

7.1: 2,6-dimethylpyridine; oxalyl dichloride / dichloromethane / 0.5 h / 0 °C

7.2: 2.5 h / 0 - 20 °C

With 2,6-dimethylpyridine; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; oxalyl dichloride; tetraethylammonium chloride; potassium acetate; phosphorus tribromide; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; tert-butyl alcohol; palladium diacetate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; 1.1: Intramolecular Heck cyclization;