C₁₉H₂₄O₃

Base Information

Chemical Name:C₁₉H₂₄O₃
CAS No.:602277-02-1
Molecular Formula:C₁₉H₂₄O₃
Molecular Weight:300.398
Hs Code.:

C<sub>19</sub>H<sub>24</sub>O<sub>3</sub>

Synonyms:C₁₉H₂₄O₃

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Chemical Property of C₁₉H₂₄O₃

Chemical Property:

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Technology Process of C₁₉H₂₄O₃

There total 6 articles about C₁₉H₂₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 591-50-4
iodobenzene

: 602277-01-0
C₁₃H₂₀O₃

: 602277-02-1
C₁₉H₂₄O₃

Guidance literature:: With tetra-(n-butyl)ammonium iodide; triethylamine; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide; at 110 ℃; for 6h;
DOI:10.1016/S0040-4039(03)01256-5

Reference yield:

: 18546-21-9
1,2:5,6-di-O-cyclohexylidene-α-D-ribo-3-hexofuranose-3-ulose

: 602277-02-1
C₁₉H₂₄O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: 67 percent / tetrahydrofuran / 0.5 h / -10 °C

2.1: 97 percent / H₂ / Pd/C / 3 h / 2585.74 Torr

3.1: 83 percent / aq. H₂SO₄ / methanol / 24 h

4.1: MsCl; NEt₃ / CH₂Cl₂ / 2 h / 0 - 20 °C

4.2: EtCOMe; NaI / CH₂Cl₂ / 6 h / Heating

5.1: 63 percent / PPh₃; NEt₃; TBAI / Pd(OAc)2 / dimethylformamide / 6 h / 110 °C

With sulfuric acid; hydrogen; tetra-(n-butyl)ammonium iodide; methanesulfonyl chloride; triethylamine; triphenylphosphine; palladium diacetate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 1.1: Wittig reaction / 5.1: Heck reaction;
DOI:10.1016/S0040-4039(03)01256-5

Reference yield:

: 23397-76-4
1,2:5,6-di-O-cyclohexylidene-α-D-glucofuranose

: 602277-02-1
C₁₉H₂₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 78 percent / PDC; 4 Angstroem MS; Ac₂O / CH₂Cl₂ / 12 h / 20 °C

2.1: 67 percent / tetrahydrofuran / 0.5 h / -10 °C

3.1: 97 percent / H₂ / Pd/C / 3 h / 2585.74 Torr

4.1: 83 percent / aq. H₂SO₄ / methanol / 24 h

5.1: MsCl; NEt₃ / CH₂Cl₂ / 2 h / 0 - 20 °C

5.2: EtCOMe; NaI / CH₂Cl₂ / 6 h / Heating

6.1: 63 percent / PPh₃; NEt₃; TBAI / Pd(OAc)2 / dimethylformamide / 6 h / 110 °C

With dipyridinium dichromate; 4 Angstroem MS; sulfuric acid; hydrogen; acetic anhydride; tetra-(n-butyl)ammonium iodide; methanesulfonyl chloride; triethylamine; triphenylphosphine; palladium diacetate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 2.1: Wittig reaction / 6.1: Heck reaction;
DOI:10.1016/S0040-4039(03)01256-5