2,3-di[(octadecylamino)carbonyl]oxypropyl (4-nitrophenyl) [11-[(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxyundecyl] phosphonate

Base Information

Chemical Name:2,3-di[(octadecylamino)carbonyl]oxypropyl (4-nitrophenyl) [11-[(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxyundecyl] phosphonate
CAS No.:305368-31-4
Molecular Formula:C₆₃H₁₁₁N₄O₁₄P
Molecular Weight:1179.57
Hs Code.:

Synonyms:2,3-di[(octadecylamino)carbonyl]oxypropyl (4-nitrophenyl) [11-[(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxyundecyl] phosphonate

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Chemical Property of 2,3-di[(octadecylamino)carbonyl]oxypropyl (4-nitrophenyl) [11-[(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxyundecyl] phosphonate

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Technology Process of 2,3-di[(octadecylamino)carbonyl]oxypropyl (4-nitrophenyl) [11-[(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxyundecyl] phosphonate

There total 3 articles about 2,3-di[(octadecylamino)carbonyl]oxypropyl (4-nitrophenyl) [11-[(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxyundecyl] phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: C₂₂H₃₀ClN₂O₉P

: (R,S)-1,2-dioctadecylcarbamoylglycerol

: 305368-31-4
2,3-di[(octadecylamino)carbonyl]oxypropyl (4-nitrophenyl) [11-[(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxyundecyl] phosphonate

Guidance literature:: With triethylamine; In dichloromethane; Heating;
DOI:10.1016/S0960-894X(00)00396-6

Reference yield:

: 268227-43-6
ethyl (4-nitrophenyl)[11-([(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxy)undecyl]phosphonate

: 305368-31-4
2,3-di[(octadecylamino)carbonyl]oxypropyl (4-nitrophenyl) [11-[(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxyundecyl] phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 48 h / 20 °C

2: (COCl)2 / CH₂Cl₂ / 2 h / 0 - 20 °C

3: 66 percent / Et₃N / CH₂Cl₂ / Heating

With oxalyl dichloride; triethylamine; In dichloromethane; 1: Silylation / 2: Chlorination / 3: Esterification;
DOI:10.1016/S0960-894X(00)00396-6

Reference yield:

: C₂₅H₃₉N₂O₁₀PSi

: 305368-31-4
2,3-di[(octadecylamino)carbonyl]oxypropyl (4-nitrophenyl) [11-[(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxyundecyl] phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: (COCl)2 / CH₂Cl₂ / 2 h / 0 - 20 °C

2: 66 percent / Et₃N / CH₂Cl₂ / Heating

With oxalyl dichloride; triethylamine; In dichloromethane; 1: Chlorination / 2: Esterification;
DOI:10.1016/S0960-894X(00)00396-6