N-pyrrolidin-(2S)-ylmethyl-benzensulfonamide trifluoroacetic acid salt

Base Information

• Chemical Name: N-pyrrolidin-(2S)-ylmethyl-benzensulfonamide trifluoroacetic acid salt
• CAS No.: 853934-69-7
• Molecular Formula: C₂HF₃O₂*C₁₁H₁₆N₂O₂S
• Molecular Weight: 354.35

Synonyms:N-pyrrolidin-(2S)-ylmethyl-benzensulfonamide trifluoroacetic acid salt

Chemical Property of N-pyrrolidin-(2S)-ylmethyl-benzensulfonamide trifluoroacetic acid salt

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Technology Process of N-pyrrolidin-(2S)-ylmethyl-benzensulfonamide trifluoroacetic acid salt

There total 1 articles about N-pyrrolidin-(2S)-ylmethyl-benzensulfonamide trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S)-(benzenesulphonylamino-methyl)-pyrrolidine-1-carboxylic acid tert-butyl ester (853934-67-5) + trifluoroacetic acid (76-05-1) → N-pyrrolidin-(2S)-ylmethyl-benzensulfonamide trifluoroacetic acid salt (853934-69-7)

Guidance literature:

In dichloromethane; at 20 ℃; for 2h;

Reference yield:

N-pyrrolidin-(2S)-ylmethyl-benzensulfonamide trifluoroacetic acid salt (853934-69-7) + [(R)-1-chlorosulphonylmethyl-2-(2-fluoro-phenyl)-ethyl]-carbamic acid tert-butyl ester (910111-78-3) → [(R)-1-[(S)-2-(benzenesulphonylamino-methyl)-pyrrolidine-1-sulphonylmethyl]-2-(2-fluoro-phenyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

N-pyrrolidin-(2S)-ylmethyl-benzensulfonamide trifluoroacetic acid salt (853934-69-7) + (1R)-[(2-fluoro-benzyl)-3-oxo-propyl]-carbamic acid tert-butyl ester (871130-55-1) → [3-[(2S)-(Benzenesulfonylamino-methyl)-pyrrolidin-1-yl]-(1R)-(2-fluoro-benzyl)-propyl]-carbamic acid tert-butylester (871130-64-2)

Guidance literature:

In dichloromethane;

upstream raw materials:

(2S)-(benzenesulphonylamino-methyl)-pyrrolidine-1-carboxylic acid tert-butyl ester

trifluoroacetic acid

Downstream raw materials:

[3-[(2S)-(Benzenesulfonylamino-methyl)-pyrrolidin-1-yl]-(1R)-(2-fluoro-benzyl)-propyl]-carbamic acid tert-butylester

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