2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten

Base Information

Chemical Name:2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten
CAS No.:1158817-46-9
Molecular Formula:C₂₅H₃₅BO₃Si
Molecular Weight:422.448
Hs Code.:

Synonyms:2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten

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Chemical Property of 2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten

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Technology Process of 2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten

There total 1 articles about 2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 915225-49-9
2-(chlorodiphenylsilyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 19781-54-5
2,4-dimethyl-1-penten-3-ol

: 1158817-46-9
2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.200805406

Reference yield: 87.0%

: 1158817-46-9
2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten

: 1158817-57-2
(E)-2,4-dimethyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(diphenylsilyloxy)pent-1-ene

Guidance literature:: With catalyst: P(4-CF₃C₆H₄)3+[Pt(dba)2]; In toluene; glass tube with PTFE stopcock charged with P(4-CF3C6H4)3, Pt(dba)2, toluene and B(pin) deriv.; tube sealed with stopcock; mixt. heated at 80°C with stirring for 3 h; volatile materials removed by evapn.; purified by silica gel column chromy. or by HPLC;
DOI:10.1002/anie.200805406