Technology Process of 2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten
There total 1 articles about 2,4-dimethyl-3-[diphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silyloxy]-1-penten which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
catalyst: P(4-CF3C6H4)3+[Pt(dba)2];
In
toluene;
glass tube with PTFE stopcock charged with P(4-CF3C6H4)3, Pt(dba)2, toluene and B(pin) deriv.; tube sealed with stopcock; mixt. heated at 80°C with stirring for 3 h; volatile materials removed by evapn.; purified by silica gel column chromy. or by HPLC;
DOI:10.1002/anie.200805406