((CH₃)3C₆H₂)2Ge(SCH(CH₃)2)P(H)C₆H₂(C(CH₃)3)3

Base Information

Chemical Name:((CH₃)3C₆H₂)2Ge(SCH(CH₃)2)P(H)C₆H₂(C(CH₃)3)3
CAS No.:106092-60-8
Molecular Formula:C₃₉H₅₉GePS
Molecular Weight:663.527
Hs Code.:

((CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>)2Ge(SCH(CH<sub>3</sub>)2)P(H)C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)3

Synonyms:((CH₃)3C₆H₂)2Ge(SCH(CH₃)2)P(H)C₆H₂(C(CH₃)3)3

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Chemical Property of ((CH₃)3C₆H₂)2Ge(SCH(CH₃)2)P(H)C₆H₂(C(CH₃)3)3

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Technology Process of ((CH₃)3C₆H₂)2Ge(SCH(CH₃)2)P(H)C₆H₂(C(CH₃)3)3

There total 3 articles about ((CH₃)3C₆H₂)2Ge(SCH(CH₃)2)P(H)C₆H₂(C(CH₃)3)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 96481-35-5
dimesitylgerma(2,4,6-tri-tert-butylphenyl)phosphene

: 75-33-2
2-propanethiol

: 106092-60-8
((CH₃)3C₆H₂)2Ge(SCH(CH₃)2)P(H)C₆H₂(C(CH₃)3)3

Guidance literature:: In pentane; addn. of equimolar amts. of reagent to a soln. of germaphosphene in pentane (N2, room temp.), decoloration of soln. occurrs immediately; evapn. (reduced pressure), recrystn. from pentane; elem. anal.;
DOI:10.1021/ja00236a016

Reference yield:

: 96481-37-7
(dimesityl)fluorogermyl(2,4,6-butylphenyl)phosphine

: 20607-43-6
sodium isopropanethiolate

: 106092-60-8
((CH₃)3C₆H₂)2Ge(SCH(CH₃)2)P(H)C₆H₂(C(CH₃)3)3

Guidance literature:: In diethyl ether; byproducts: NaF; addn. of a soln. of i-PrSNa to a soln. of Ge-compd. in diethyl ether, heating at 35°C for 1 h (N2); filtration, evapn., recrystn. of residue in pentane;
DOI:10.1021/ja00236a016

Reference yield:

: 96481-35-5
dimesitylgerma(2,4,6-tri-tert-butylphenyl)phosphene

: 106092-60-8
((CH₃)3C₆H₂)2Ge(SCH(CH₃)2)P(H)C₆H₂(C(CH₃)3)3

Guidance literature:: With NaBH₄; In tetrahydrofuran; water; the Mn-complex was treated with NaBH4 in H2O/THF under N2, then an aq. soln. of n-Bu4NBr was added;; THF was removed, the resulting oil was not further purified;;
DOI:10.1016/0022-328X(85)80048-6