C₁₅H₁₁BrCl₂N₂O₂

Base Information

Chemical Name:C₁₅H₁₁BrCl₂N₂O₂
CAS No.:845752-06-9
Molecular Formula:C₁₅H₁₁BrCl₂N₂O₂
Molecular Weight:402.075
Hs Code.:

C<sub>15</sub>H<sub>11</sub>BrCl<sub>2</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₅H₁₁BrCl₂N₂O₂

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Chemical Property of C₁₅H₁₁BrCl₂N₂O₂

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Technology Process of C₁₅H₁₁BrCl₂N₂O₂

There total 6 articles about C₁₅H₁₁BrCl₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 845752-05-8
C₁₅H₁₀Br₂Cl₂N₂O₂

: 845752-06-9
C₁₅H₁₁BrCl₂N₂O₂

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; at 20 ℃; for 8h;

Reference yield:

: 5435-54-1
4-hydroxy-3-nitropyridine

: 845752-06-9
C₁₅H₁₁BrCl₂N₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: phosphorus pentachloride; trichlorophosphate / 5 h / 70 - 140 °C

2: dipotassium hydrogenphosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / DMF (N,N-dimethyl-formamide); water / 21 h / 68 °C

3: hydrogenchloride; iron / ethanol; water / 2 h / 90 °C

4: bromine; acetic acid / 23 h / 20 °C

5: methanesulfonic acid / 130 °C

6: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 8 h / 20 °C

With hydrogenchloride; dipotassium hydrogenphosphate; methanesulfonic acid; phosphorus pentachloride; hydrogen; bromine; iron; acetic acid; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; water;

Reference yield:

: 845752-03-6
C₁₁H₈Cl₂N₂

: 845752-06-9
C₁₅H₁₁BrCl₂N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: bromine; acetic acid / 23 h / 20 °C

2: methanesulfonic acid / 130 °C

3: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 8 h / 20 °C

With methanesulfonic acid; hydrogen; bromine; acetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol;