(2E,6E)-10-bromo-1-((tert-butyldiphenylsilyl)oxy)-11-hydroxy-3,7,11-trimethyl-2,6-dodecadiene

Base Information

Chemical Name:(2E,6E)-10-bromo-1-((tert-butyldiphenylsilyl)oxy)-11-hydroxy-3,7,11-trimethyl-2,6-dodecadiene
CAS No.:151409-32-4
Molecular Formula:C₃₁H₄₅BrO₂Si
Molecular Weight:557.687
Hs Code.:

Synonyms:(2E,6E)-10-bromo-1-((tert-butyldiphenylsilyl)oxy)-11-hydroxy-3,7,11-trimethyl-2,6-dodecadiene

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Chemical Property of (2E,6E)-10-bromo-1-((tert-butyldiphenylsilyl)oxy)-11-hydroxy-3,7,11-trimethyl-2,6-dodecadiene

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Technology Process of (2E,6E)-10-bromo-1-((tert-butyldiphenylsilyl)oxy)-11-hydroxy-3,7,11-trimethyl-2,6-dodecadiene

There total 3 articles about (2E,6E)-10-bromo-1-((tert-butyldiphenylsilyl)oxy)-11-hydroxy-3,7,11-trimethyl-2,6-dodecadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 151409-23-3
tert-butyldiphenyl {[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl]oxy}silane

: 151409-32-4
(2E,6E)-10-bromo-1-((tert-butyldiphenylsilyl)oxy)-11-hydroxy-3,7,11-trimethyl-2,6-dodecadiene

Guidance literature:: With N-Bromosuccinimide; water; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1002/jlcr.2580361106

Reference yield:

: 106-28-5
Farnesol

: 151409-32-4
(2E,6E)-10-bromo-1-((tert-butyldiphenylsilyl)oxy)-11-hydroxy-3,7,11-trimethyl-2,6-dodecadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / dichloromethane / 1 h / 0 °C

2: N-Bromosuccinimide; water / tetrahydrofuran / 2 h / 0 °C

With 1H-imidazole; N-Bromosuccinimide; water; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm5009456

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 151409-32-4
(2E,6E)-10-bromo-1-((tert-butyldiphenylsilyl)oxy)-11-hydroxy-3,7,11-trimethyl-2,6-dodecadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / dichloromethane / 1 h / 0 °C

2: N-Bromosuccinimide; water / tetrahydrofuran / 2 h / 0 °C

With 1H-imidazole; N-Bromosuccinimide; water; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm5009456