(2R,3S,4S)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone

Base Information

Chemical Name:(2R,3S,4S)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone
CAS No.:110612-41-4
Molecular Formula:C₂₆H₄₀O₃
Molecular Weight:400.602
Hs Code.:

Synonyms:(2R,3S,4S)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone

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Chemical Property of (2R,3S,4S)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone

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Technology Process of (2R,3S,4S)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone

There total 5 articles about (2R,3S,4S)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 110560-68-4
(2R,3S,4R)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone

: 110612-41-4
(2R,3S,4S)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone

Guidance literature:: With triethylamine; for 1h; Ambient temperature;
DOI:10.1002/hlca.19860690813

Reference yield:

: 110560-76-4
2-(methyloxy)propionic acid

: 110612-41-4
(2R,3S,4S)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / SOCl₂

2: 50 percent / Et₃N / neat (no solvent) / 3 h / Ambient temperature

3: 95 percent / Et₃N / 1 h / Ambient temperature

With thionyl chloride; triethylamine; In neat (no solvent);
DOI:10.1002/hlca.19860690813

Reference yield:

: 27303-99-7
sodium menthoxide

: 110612-41-4
(2R,3S,4S)-3-Benzyloxy-4-butyl-2-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyloxy)-2-methyl-cyclobutanone

Guidance literature:: Multi-step reaction with 5 steps

1: dimethylformamide

2: KOH / methanol

3: 77 percent / SOCl₂

4: 50 percent / Et₃N / neat (no solvent) / 3 h / Ambient temperature

5: 95 percent / Et₃N / 1 h / Ambient temperature

With potassium hydroxide; thionyl chloride; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19860690813