Technology Process of C23H23NO5
There total 6 articles about C23H23NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid;
In
chloroform;
at 150 ℃;
for 0.333333h;
regioselective reaction;
Inert atmosphere;
Microwave irradiation;
DOI:10.1021/ol3008588
- Guidance literature:
-
Multi-step reaction with 2 steps
1: silver(I) acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 1 h / 20 °C / Inert atmosphere; Darkness
2: acetic acid / chloroform / 0.33 h / 150 °C / Inert atmosphere; Microwave irradiation
With
silver(I) acetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
chloroform; acetonitrile;
DOI:10.1021/ol3008588
- Guidance literature:
-
Multi-step reaction with 3 steps
1: magnesium sulfate; triethylamine / dichloromethane
2: silver(I) acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 1 h / 20 °C / Inert atmosphere; Darkness
3: trifluoroacetic acid / chloroform / 0.67 h / 110 °C / Microwave irradiation
With
silver(I) acetate; magnesium sulfate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid;
In
dichloromethane; chloroform; acetonitrile;
DOI:10.1021/acs.joc.0c01256