trans-1-acetoxy-2-<<(methylsulfonyl)oxy>ethyl>-1,3,3-trimethylcyclohexane

Base Information

Chemical Name:trans-1-acetoxy-2-<<(methylsulfonyl)oxy>ethyl>-1,3,3-trimethylcyclohexane
CAS No.:142763-03-9
Molecular Formula:C₁₄H₂₆O₅S
Molecular Weight:306.423
Hs Code.:

Synonyms:trans-1-acetoxy-2-<<(methylsulfonyl)oxy>ethyl>-1,3,3-trimethylcyclohexane

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Chemical Property of trans-1-acetoxy-2-<<(methylsulfonyl)oxy>ethyl>-1,3,3-trimethylcyclohexane

Chemical Property:

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Technology Process of trans-1-acetoxy-2-<<(methylsulfonyl)oxy>ethyl>-1,3,3-trimethylcyclohexane

There total 2 articles about trans-1-acetoxy-2-<<(methylsulfonyl)oxy>ethyl>-1,3,3-trimethylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64532-88-3,71041-58-2,100534-08-5
trans-2-(2-hydroxyethyl)-1,3,3-trimethylcyclohexan-1-ol

: 142763-03-9
trans-1-acetoxy-2-<<(methylsulfonyl)oxy>ethyl>-1,3,3-trimethylcyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / N,N-diethylaniline / CHCl₃ / 7 h / Heating

2: 50 percent / K₂CO₃ / methanol; H₂O / 4.5 h / 0 °C

3: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With potassium carbonate; triethylamine; N,N-diethylaniline; In methanol; dichloromethane; chloroform; water;
DOI:10.1021/jo00044a024

Reference yield:

: 101106-98-3,142763-01-7
trans-1-acetoxy-2-(2-acetoxyethyl)-1,3,3-trimethylcyclohexane

: 142763-03-9
trans-1-acetoxy-2-<<(methylsulfonyl)oxy>ethyl>-1,3,3-trimethylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / K₂CO₃ / methanol; H₂O / 4.5 h / 0 °C

2: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With potassium carbonate; triethylamine; In methanol; dichloromethane; water;
DOI:10.1021/jo00044a024